2,5-di-O-mesyl-3,4-di-O-p-methoxybenzyl-1,6-di-O-tert-butyldimethylsilyl-D-mannitol

Base Information

Chemical Name:2,5-di-O-mesyl-3,4-di-O-p-methoxybenzyl-1,6-di-O-tert-butyldimethylsilyl-D-mannitol
CAS No.:1235554-95-6
Molecular Formula:C₃₆H₆₂O₁₂S₂Si₂
Molecular Weight:807.184
Hs Code.:

Synonyms:2,5-di-O-mesyl-3,4-di-O-p-methoxybenzyl-1,6-di-O-tert-butyldimethylsilyl-D-mannitol

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Chemical Property of 2,5-di-O-mesyl-3,4-di-O-p-methoxybenzyl-1,6-di-O-tert-butyldimethylsilyl-D-mannitol

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Technology Process of 2,5-di-O-mesyl-3,4-di-O-p-methoxybenzyl-1,6-di-O-tert-butyldimethylsilyl-D-mannitol

There total 1 articles about 2,5-di-O-mesyl-3,4-di-O-p-methoxybenzyl-1,6-di-O-tert-butyldimethylsilyl-D-mannitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1235554-94-5
3,4-di-O-p-methoxbenzyl-1,6-di-O-tert-butyldimethylsilyl-D-mannitol

: 124-63-0
methanesulfonyl chloride

: 1235554-95-6
2,5-di-O-mesyl-3,4-di-O-p-methoxybenzyl-1,6-di-O-tert-butyldimethylsilyl-D-mannitol

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; Inert atmosphere;
DOI:10.1071/CH09426

Reference yield:

: 1235554-95-6
2,5-di-O-mesyl-3,4-di-O-p-methoxybenzyl-1,6-di-O-tert-butyldimethylsilyl-D-mannitol

: C₂₄H₃₄O₁₂S₂

Guidance literature:: With hydrogenchloride; water; In methanol; at 0 ℃;
DOI:10.1071/CH09426

Reference yield:

: 1235554-95-6
2,5-di-O-mesyl-3,4-di-O-p-methoxybenzyl-1,6-di-O-tert-butyldimethylsilyl-D-mannitol

: 1235554-91-2
1,2:5,6-dianhydro-3,4-di-O-p-methoxybenzyl-L-iditol

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; water / methanol / 0 °C

2: water; potassium hydroxide / methanol / 20 °C

With hydrogenchloride; water; potassium hydroxide; In methanol;
DOI:10.1071/CH09426