L-glutamic acid α-benzyl ester γ-n-butylamide p-toluenesulfonate salt

Base Information

Chemical Name:L-glutamic acid α-benzyl ester γ-n-butylamide p-toluenesulfonate salt
CAS No.:79640-79-2
Molecular Formula:C₇H₈O₃S*C₁₆H₂₄N₂O₃
Molecular Weight:464.583
Hs Code.:

Synonyms:L-glutamic acid α-benzyl ester γ-n-butylamide p-toluenesulfonate salt

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Chemical Property of L-glutamic acid α-benzyl ester γ-n-butylamide p-toluenesulfonate salt

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Technology Process of L-glutamic acid α-benzyl ester γ-n-butylamide p-toluenesulfonate salt

There total 2 articles about L-glutamic acid α-benzyl ester γ-n-butylamide p-toluenesulfonate salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 104-15-4
toluene-4-sulfonic acid

: 79640-73-6
N-(tert-butyloxycarbonyl)-L-glutamic acid α-benzyl ester γ-n-butylamide

: 79640-79-2
L-glutamic acid α-benzyl ester γ-n-butylamide p-toluenesulfonate salt

Guidance literature:: In benzene; for 0.75h; Heating;
DOI:10.1021/jm00144a016

Reference yield:

: 30924-93-7
Boc-Glu-OBn

: 79640-79-2
L-glutamic acid α-benzyl ester γ-n-butylamide p-toluenesulfonate salt

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / diphenylphosphoryl azide, Et₃N / dimethylformamide / 1.) 0 deg C, 6 h, 2.) RT, overnight

2: 98 percent / benzene / 0.75 h / Heating

With diphenylphosphoranyl azide; triethylamine; In N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm00144a016

Reference yield:

: 19741-14-1
4-[(2,4-diaminopteridin-6-ylmethyl)methylamino]benzoic acid

: 79640-79-2
L-glutamic acid α-benzyl ester γ-n-butylamide p-toluenesulfonate salt

: 79640-71-4
methotrexate α-benzyl ester γ-n-butylamide

Guidance literature:: With diethyl cyanophosphonate; triethylamine; Yield given. Multistep reaction; 1.) DMF, 80 deg C, 2 min, 2.) DMF, 80 deg C, 2 h;
DOI:10.1021/jm00144a016