Methyl 2-deoxy-3-O-methyl-4-O-methanesulfonyl-6-O-triphenylmethyl-α-D-arabino-hexopyranoside

Base Information

Chemical Name:Methyl 2-deoxy-3-O-methyl-4-O-methanesulfonyl-6-O-triphenylmethyl-α-D-arabino-hexopyranoside
CAS No.:126257-14-5
Molecular Formula:C₂₈H₃₂O₇S
Molecular Weight:512.624
Hs Code.:

Synonyms:Methyl 2-deoxy-3-O-methyl-4-O-methanesulfonyl-6-O-triphenylmethyl-α-D-arabino-hexopyranoside

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Chemical Property of Methyl 2-deoxy-3-O-methyl-4-O-methanesulfonyl-6-O-triphenylmethyl-α-D-arabino-hexopyranoside

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Technology Process of Methyl 2-deoxy-3-O-methyl-4-O-methanesulfonyl-6-O-triphenylmethyl-α-D-arabino-hexopyranoside

There total 7 articles about Methyl 2-deoxy-3-O-methyl-4-O-methanesulfonyl-6-O-triphenylmethyl-α-D-arabino-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 126257-19-0
Methyl 2-deoxy-3-O-methyl-6-O-triphenylmethyl-α-D-arabino-hexopyranoside

: 124-63-0
methanesulfonyl chloride

: 126257-14-5
Methyl 2-deoxy-3-O-methyl-4-O-methanesulfonyl-6-O-triphenylmethyl-α-D-arabino-hexopyranoside

Guidance literature:: With pyridine; In chloroform; for 24h; Ambient temperature;
DOI:10.1021/jo00298a033

Reference yield:

: 126373-46-4
4,6-O-Benzylidene-2-deoxy-3-O-methyl-α-D-arabino-hexopyranoside

: 126257-14-5
Methyl 2-deoxy-3-O-methyl-4-O-methanesulfonyl-6-O-triphenylmethyl-α-D-arabino-hexopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / H₂, acetic acid / 10percent Pd/C / methanol / 2.5 h / 760 Torr

2: 16.31 g / pyridine / 120 h / Ambient temperature

3: 73 percent / pyridine / CHCl₃ / 24 h / Ambient temperature

With pyridine; hydrogen; acetic acid; palladium on activated charcoal; In methanol; chloroform;
DOI:10.1021/jo00298a033

Reference yield:

: 16718-95-9
methyl 4,6-O-benzylidene-2-deoxy-α-D-altropyranoside

: 126257-14-5
Methanesulfonic acid (2R,3S,4S,6S)-4,6-dimethoxy-2-trityloxymethyl-tetrahydro-pyran-3-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / tetrahydrofuran / Ambient temperature

2: hydrogen / 10percent Pd-C

4: pyridine

With pyridine; hydrogen; sodium hydride; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1016/0008-6215(86)84026-5