malBel

Base Information

Chemical Name:malBel
CAS No.:1262297-34-6
Molecular Formula:C₁₉H₁₈N₂O₈S
Molecular Weight:434.427
Hs Code.:

Synonyms:malBel

Suppliers and Price of malBel

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of malBel

Chemical Property:

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Technology Process of malBel

There total 9 articles about malBel which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1262297-42-6
C₂₁H₂₂N₂O₈S

: 1262297-34-6
malBel

Guidance literature:: C₂₁H₂₂N₂O₈S; With water; sodium hydroxide; In methanol; at 75 ℃; for 1h;

With hydrogenchloride; In water;

Reference yield:

: 38323-22-7
dimethyl (4-nitrobenzylidene)malonate

: 1262297-34-6
malBel

Guidance literature:: Multi-step reaction with 6 steps

1: sodium cyanoborohydride / methanol / 20 °C

2: hydrogen / palladium 10% on activated carbon / methanol / 20 °C

3: pyridine / dichloromethane / 1 h / 40 °C

4: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / Reflux

5: hydroxylamine hydrochloride; sodium hydrogencarbonate / tetrahydrofuran / 1 h / 20 °C

6: sodium hydroxide; water / methanol / 1 h / 75 °C

With pyridine; oxalyl dichloride; hydroxylamine hydrochloride; water; hydrogen; sodium cyanoborohydride; sodium hydrogencarbonate; sodium hydroxide; palladium 10% on activated carbon; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 1262297-34-6
malBel

Guidance literature:: Multi-step reaction with 7 steps

1: piperidine; benzoic acid / ethanol / 5 h / Reflux

2: sodium cyanoborohydride / methanol / 20 °C

3: hydrogen / palladium 10% on activated carbon / methanol / 20 °C

4: pyridine / dichloromethane / 1 h / 40 °C

5: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / Reflux

6: hydroxylamine hydrochloride; sodium hydrogencarbonate / tetrahydrofuran / 1 h / 20 °C

7: sodium hydroxide; water / methanol / 1 h / 75 °C

With piperidine; pyridine; oxalyl dichloride; hydroxylamine hydrochloride; water; hydrogen; sodium cyanoborohydride; sodium hydrogencarbonate; benzoic acid; sodium hydroxide; palladium 10% on activated carbon; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; ethanol; dichloromethane;