N-((4aR,6R,7R,8R,8aS)-6-Cyclohexyloxy-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-acetamide

Base Information

Chemical Name:N-((4aR,6R,7R,8R,8aS)-6-Cyclohexyloxy-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-acetamide
CAS No.:197574-97-3
Molecular Formula:C₂₁H₂₉NO₆
Molecular Weight:391.464
Hs Code.:

Synonyms:N-((4aR,6R,7R,8R,8aS)-6-Cyclohexyloxy-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-acetamide

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Chemical Property of N-((4aR,6R,7R,8R,8aS)-6-Cyclohexyloxy-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-acetamide

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Technology Process of N-((4aR,6R,7R,8R,8aS)-6-Cyclohexyloxy-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-acetamide

There total 4 articles about N-((4aR,6R,7R,8R,8aS)-6-Cyclohexyloxy-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 21559-72-8
cyclohexyl 2-(acetylamino)-2-deoxy-β-D-glucopyranoside

: 1125-88-8
benzaldehyde dimethyl acetal

: 197574-97-3
N-((4aR,6R,7R,8R,8aS)-6-Cyclohexyloxy-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-acetamide

Guidance literature:: With sulfuric acid; In 1,4-dioxane; methanol; at 90 - 95 ℃; for 0.0833333h;
DOI:10.1007/BF02273926

Reference yield:

: 21588-60-3
cyclohexyl 3,4,6-tri-O-acetyl-2-(acetylamino)-2-deoxy-β-D-glucopyranoside

: 197574-97-3
N-((4aR,6R,7R,8R,8aS)-6-Cyclohexyloxy-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / CH₃ONa / methanol

2: 78 percent / H₂SO₄ / dioxane; methanol / 0.08 h / 90 - 95 °C

With sulfuric acid; sodium methylate; In 1,4-dioxane; methanol;
DOI:10.1007/BF02273926

Reference yield:

: 108-93-0
cyclohexanol

: 197574-97-3
N-((4aR,6R,7R,8R,8aS)-6-Cyclohexyloxy-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / HgI₂, 3 Angstroem molecular sieves / CH₂Cl₂

2: 96 percent / CH₃ONa / methanol

3: 78 percent / H₂SO₄ / dioxane; methanol / 0.08 h / 90 - 95 °C

With 3 A molecular sieve; sulfuric acid; sodium methylate; mercury(II) iodide; In 1,4-dioxane; methanol; dichloromethane;
DOI:10.1007/BF02273926