1,2-O-[12-[N-(4-azido-2,3,5,6-tetrafluorobenzoyl)]aminododecanoyl]-2-lyso-sn-glycero-3-phosphocholine

Base Information

• Chemical Name: 1,2-O-[12-[N-(4-azido-2,3,5,6-tetrafluorobenzoyl)]aminododecanoyl]-2-lyso-sn-glycero-3-phosphocholine
• CAS No.: 423756-22-3
• Molecular Formula: C₂₇H₄₂F₄N₅O₈P
• Molecular Weight: 671.627

Synonyms:1,2-O-[12-[N-(4-azido-2,3,5,6-tetrafluorobenzoyl)]aminododecanoyl]-2-lyso-sn-glycero-3-phosphocholine

Chemical Property of 1,2-O-[12-[N-(4-azido-2,3,5,6-tetrafluorobenzoyl)]aminododecanoyl]-2-lyso-sn-glycero-3-phosphocholine

Chemical Property:

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Technology Process of 1,2-O-[12-[N-(4-azido-2,3,5,6-tetrafluorobenzoyl)]aminododecanoyl]-2-lyso-sn-glycero-3-phosphocholine

There total 1 articles about 1,2-O-[12-[N-(4-azido-2,3,5,6-tetrafluorobenzoyl)]aminododecanoyl]-2-lyso-sn-glycero-3-phosphocholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

1,2-O-di[12-[N-(4-azido-2,3,5,6-tetrafluorobenzoyl)]aminododecanoyl]-sn-glycero-3-phosphocholine (423756-21-2) → 1,2-O-[12-[N-(4-azido-2,3,5,6-tetrafluorobenzoyl)]aminododecanoyl]-2-lyso-sn-glycero-3-phosphocholine (423756-22-3)

Guidance literature:

With phospholipase A₂; In methanol; at 38 ℃;

DOI:10.1021/jm011032f

Reference yield: 94.0%

oleic anhydride (6085-36-5,55726-25-5,24909-72-6) + 1,2-O-[12-[N-(4-azido-2,3,5,6-tetrafluorobenzoyl)]aminododecanoyl]-2-lyso-sn-glycero-3-phosphocholine (423756-22-3) → 1-O-[12-[N-(4-azido-2,3,5,6-tetrafluorobenzoyl)]aminododecanoyl]-2-oleoyl-sn-glycero-3-phosphocholine (423756-23-4)

Guidance literature:

In chloroform; benzene; at 20 ℃; for 5h;

DOI:10.1021/jm011032f

Reference yield:

1,2-O-[12-[N-(4-azido-2,3,5,6-tetrafluorobenzoyl)]aminododecanoyl]-2-lyso-sn-glycero-3-phosphocholine (423756-22-3) → 1-O-[12-[N-(4-azido-2,3,5,6-tetrafluorobenzoyl)]aminododecanoyl]-2-oleoyl-sn-glycero-3-phosphoate

Guidance literature:

Multi-step reaction with 2 steps

1: 94 percent / benzene; CHCl₃ / 5 h / 20 °C

2: 61 percent / CH₃COONa; CaCl₂; phospholipase D / diethyl ether / 30 - 35 °C / sonication

With sodium acetate; calcium chloride; phospholipase D; In diethyl ether; chloroform; benzene;

DOI:10.1021/jm011032f

upstream raw materials:

1,2-O-di[12-[N-(4-azido-2,3,5,6-tetrafluorobenzoyl)]aminododecanoyl]-sn-glycero-3-phosphocholine

Downstream raw materials:

1-O-[12-[N-(4-azido-2,3,5,6-tetrafluorobenzoyl)]aminododecanoyl]-2-oleoyl-sn-glycero-3-phosphocholine

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