4-(carboxymethyl)-1-phenyl-1,4-dihydropyridine-3,5-dicarb-oxylic acid

Base Information

Chemical Name:4-(carboxymethyl)-1-phenyl-1,4-dihydropyridine-3,5-dicarb-oxylic acid
CAS No.:1418218-56-0
Molecular Formula:C₁₅H₁₃NO₆
Molecular Weight:303.271
Hs Code.:

Synonyms:4-(carboxymethyl)-1-phenyl-1,4-dihydropyridine-3,5-dicarb-oxylic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(carboxymethyl)-1-phenyl-1,4-dihydropyridine-3,5-dicarb-oxylic acid

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Technology Process of 4-(carboxymethyl)-1-phenyl-1,4-dihydropyridine-3,5-dicarb-oxylic acid

There total 3 articles about 4-(carboxymethyl)-1-phenyl-1,4-dihydropyridine-3,5-dicarb-oxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: diethyl 4-(2-ethoxy-2-oxoethyl)-1-phenyl-1,4-dihydropyridine-3,5-dicarboxylate

: 1418218-56-0
4-(carboxymethyl)-1-phenyl-1,4-dihydropyridine-3,5-dicarb-oxylic acid

Guidance literature:: With water; potassium hydroxide; In tetrahydrofuran; ethanol; at 70 ℃;
DOI:10.1016/j.tet.2012.11.094

Reference yield:

: 62-53-3
aniline

: 1418218-56-0
4-(carboxymethyl)-1-phenyl-1,4-dihydropyridine-3,5-dicarb-oxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 20 °C

2: titanium tetrachloride / dichloromethane / 20 °C

3: potassium hydroxide; water / tetrahydrofuran; ethanol / 70 °C

With water; titanium tetrachloride; potassium hydroxide; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/j.tet.2012.11.094

Reference yield:

: 15179-92-7
3-Anilinoacrylsaeure-ethylester

: 1418218-56-0
4-(carboxymethyl)-1-phenyl-1,4-dihydropyridine-3,5-dicarb-oxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: titanium tetrachloride / dichloromethane / 20 °C

2: potassium hydroxide; water / tetrahydrofuran; ethanol / 70 °C

With water; titanium tetrachloride; potassium hydroxide; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/j.tet.2012.11.094