C₁₄H₁₃BrF₃N₃

Base Information

Chemical Name:C₁₄H₁₃BrF₃N₃
CAS No.:1262198-14-0
Molecular Formula:C₁₄H₁₃BrF₃N₃
Molecular Weight:360.177
Hs Code.:

C<sub>14</sub>H<sub>13</sub>BrF<sub>3</sub>N<sub>3</sub>

Synonyms:C₁₄H₁₃BrF₃N₃

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Chemical Property of C₁₄H₁₃BrF₃N₃

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Technology Process of C₁₄H₁₃BrF₃N₃

There total 8 articles about C₁₄H₁₃BrF₃N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1420205-97-5
C₁₄H₁₅F₃N₄

: 1262198-14-0
C₁₄H₁₃BrF₃N₃

Guidance literature:: C₁₄H₁₅F₃N₄; With hydrogen bromide; sodium nitrite; In water; at 0 - 20 ℃;

With copper(I) bromide; In water; at 0 - 20 ℃;

Reference yield:

: 66417-30-9
2-bromo-1-methyl-4-(trifluoromethyl)benzene

: 1262198-14-0
C₁₄H₁₃BrF₃N₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / N,N-dimethyl-formamide / 0.17 h / 150 °C / Microwave irradiation

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 0.17 h / 150 °C / Microwave irradiation

3.1: palladium 10% on activated carbon; hydrogen / methanol; isopropyl alcohol / 50 °C / Inert atmosphere

4.1: hydrogen bromide; sodium nitrite / water / 0 - 20 °C

4.2: 0 - 20 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; hydrogen bromide; hydrogen; potassium acetate; sodium nitrite; In methanol; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; isopropyl alcohol; 2.1: |Suzuki Coupling;

Reference yield:

: 1124383-00-1
N-(3-bromo-2-pyridinyl)-N’-carboethoxy-thiourea

: 1262198-14-0
C₁₄H₁₃BrF₃N₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydroxylamine hydrochloride; N-ethyl-N,N-diisopropylamine / methanol; ethanol / 6 h / 20 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 0.17 h / 150 °C / Microwave irradiation

3.1: palladium 10% on activated carbon; hydrogen / methanol; isopropyl alcohol / 50 °C / Inert atmosphere

4.1: hydrogen bromide; sodium nitrite / water / 0 - 20 °C

4.2: 0 - 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; hydroxylamine hydrochloride; hydrogen bromide; hydrogen; N-ethyl-N,N-diisopropylamine; sodium nitrite; In methanol; 1,2-dimethoxyethane; ethanol; water; isopropyl alcohol; 2.1: |Suzuki Coupling;