Technology Process of C46H63N3O26
There total 10 articles about C46H63N3O26 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
for 3h;
Ambient temperature;
DOI:10.1039/cc9960000201
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 80 percent / BF3*Et2O / CH2Cl2 / 6 h / Ambient temperature
2: aq. KOH / ethanol / 6 h / Heating
3: 90 percent / DCC / CH2Cl2 / 1 h / Ambient temperature
4: H2 / 10percent Pd/C / methanol / 1 h
5: 65 percent / DIPEA / acetonitrile / 3 h / Ambient temperature
6: 85 percent / DCC / CH2Cl2 / 3 h / Ambient temperature
7: 94 percent / TFA / CH2Cl2 / 3 h / Ambient temperature
With
potassium hydroxide; boron trifluoride diethyl etherate; hydrogen; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid;
palladium on activated charcoal;
In
methanol; ethanol; dichloromethane; acetonitrile;
DOI:10.1039/cc9960000201
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 90 percent / DCC / CH2Cl2 / 1 h / Ambient temperature
2: H2 / 10percent Pd/C / methanol / 1 h
3: 65 percent / DIPEA / acetonitrile / 3 h / Ambient temperature
4: 85 percent / DCC / CH2Cl2 / 3 h / Ambient temperature
5: 94 percent / TFA / CH2Cl2 / 3 h / Ambient temperature
With
hydrogen; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid;
palladium on activated charcoal;
In
methanol; dichloromethane; acetonitrile;
DOI:10.1039/cc9960000201
