3-N-benzoyl-3',5'-di-O-benzoyl-5-(5-methanesulfonyloxypentyl)-2'-deoxyuridine

Base Information

• Chemical Name: 3-N-benzoyl-3',5'-di-O-benzoyl-5-(5-methanesulfonyloxypentyl)-2'-deoxyuridine
• CAS No.: 1058146-52-3
• Molecular Formula: C₃₆H₃₆N₂O₁₁S
• Molecular Weight: 704.755

Synonyms:3-N-benzoyl-3',5'-di-O-benzoyl-5-(5-methanesulfonyloxypentyl)-2'-deoxyuridine

Chemical Property of 3-N-benzoyl-3',5'-di-O-benzoyl-5-(5-methanesulfonyloxypentyl)-2'-deoxyuridine

Chemical Property:

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Technology Process of 3-N-benzoyl-3',5'-di-O-benzoyl-5-(5-methanesulfonyloxypentyl)-2'-deoxyuridine

There total 1 articles about 3-N-benzoyl-3',5'-di-O-benzoyl-5-(5-methanesulfonyloxypentyl)-2'-deoxyuridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

3-N-benzoyl-3',5'-di-O-benzoyl-5-(5-hydroxypentyl)-2'-deoxyuridine (1058146-47-6) + methanesulfonyl chloride (124-63-0) → 3-N-benzoyl-3',5'-di-O-benzoyl-5-(5-methanesulfonyloxypentyl)-2'-deoxyuridine (1058146-52-3)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 2.66667h; Inert atmosphere;

DOI:10.1021/jm800501d

Reference yield:

3-N-benzoyl-3',5'-di-O-benzoyl-5-(5-methanesulfonyloxypentyl)-2'-deoxyuridine (1058146-52-3) → C35H33(18)FN2O8 (1146730-86-0)

Guidance literature:

With [¹⁸F]-potassium fluoride; potassium carbonate; [2.2.2]cryptande;

DOI:10.1021/jo800444y

upstream raw materials:

3-N-benzoyl-3',5'-di-O-benzoyl-5-(5-hydroxypentyl)-2'-deoxyuridine

methanesulfonyl chloride

Downstream raw materials:

C₃₅H₃₃⁽¹⁸⁾FN₂O₈

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