(E)-4-(2-(3-(4-nitrophenylsulfonyl)-2-oxo-1,3-oxazinan-4-yl)vinyl)benzaldehyde

Base Information

Chemical Name:(E)-4-(2-(3-(4-nitrophenylsulfonyl)-2-oxo-1,3-oxazinan-4-yl)vinyl)benzaldehyde
CAS No.:1361394-39-9
Molecular Formula:C₁₉H₁₆N₂O₇S
Molecular Weight:416.411
Hs Code.:

Synonyms:(E)-4-(2-(3-(4-nitrophenylsulfonyl)-2-oxo-1,3-oxazinan-4-yl)vinyl)benzaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-4-(2-(3-(4-nitrophenylsulfonyl)-2-oxo-1,3-oxazinan-4-yl)vinyl)benzaldehyde

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Technology Process of (E)-4-(2-(3-(4-nitrophenylsulfonyl)-2-oxo-1,3-oxazinan-4-yl)vinyl)benzaldehyde

There total 2 articles about (E)-4-(2-(3-(4-nitrophenylsulfonyl)-2-oxo-1,3-oxazinan-4-yl)vinyl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1185060-58-5
(+/-)-3-(4-nitrophenylsulfonyl)-4-vinyl-1,3-oxazinan-2-one

: 87199-17-5
4-formylphenylboronic acid,

: 1361394-39-9
(E)-4-(2-(3-(4-nitrophenylsulfonyl)-2-oxo-1,3-oxazinan-4-yl)vinyl)benzaldehyde

Guidance literature:: With acetic acid; p-benzoquinone; In 1,2-dichloro-ethane; at 20 - 45 ℃; for 12h; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1021/ol300063t

Reference yield:

: 1185059-94-2
pent-4-enyl 4-nitrophenylsulfonylcarbamate

: 1361394-39-9
(E)-4-(2-(3-(4-nitrophenylsulfonyl)-2-oxo-1,3-oxazinan-4-yl)vinyl)benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: [1,2-bis-(phenylsulfinyl)ethane]palladium(II) acetate; 1,2-Bis(phenylsulfinyl)ethane; 2-phenyl-1,4-benzoquinone; 4-nitro-benzoic acid / 1,2-dichloro-ethane / 12 h / 45 °C

2: acetic acid; p-benzoquinone / 1,2-dichloro-ethane / 12 h / 20 - 45 °C / Inert atmosphere

With [1,2-bis-(phenylsulfinyl)ethane]palladium(II) acetate; 1,2-Bis(phenylsulfinyl)ethane; acetic acid; 2-phenyl-1,4-benzoquinone; p-benzoquinone; 4-nitro-benzoic acid; In 1,2-dichloro-ethane; 2: Heck reaction;
DOI:10.1021/ol300063t