Acetic acid 1-[2-(benzyl-trimethylsilanylmethyl-amino)-ethyl]-cyclohexa-2,5-dienylmethyl ester

Base Information

Chemical Name:Acetic acid 1-[2-(benzyl-trimethylsilanylmethyl-amino)-ethyl]-cyclohexa-2,5-dienylmethyl ester
CAS No.:143957-53-3
Molecular Formula:C₂₂H₃₃NO₂Si
Molecular Weight:371.595
Hs Code.:

Synonyms:Acetic acid 1-[2-(benzyl-trimethylsilanylmethyl-amino)-ethyl]-cyclohexa-2,5-dienylmethyl ester

Suppliers and Price of Acetic acid 1-[2-(benzyl-trimethylsilanylmethyl-amino)-ethyl]-cyclohexa-2,5-dienylmethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Acetic acid 1-[2-(benzyl-trimethylsilanylmethyl-amino)-ethyl]-cyclohexa-2,5-dienylmethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Acetic acid 1-[2-(benzyl-trimethylsilanylmethyl-amino)-ethyl]-cyclohexa-2,5-dienylmethyl ester

There total 3 articles about Acetic acid 1-[2-(benzyl-trimethylsilanylmethyl-amino)-ethyl]-cyclohexa-2,5-dienylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 30889-20-4
methyl cyclohexa-2,5-diene-1-carboxylate

: 143957-53-3
Acetic acid 1-[2-(benzyl-trimethylsilanylmethyl-amino)-ethyl]-cyclohexa-2,5-dienylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 1.5 h, 2.) a) -78 deg C, b) 25 deg C, 12 h

2: LiAlH₄ / tetrahydrofuran / 0.17 h / Heating

3: Et₃N / CH₂Cl₂ / 1 h / 25 °C

With lithium aluminium tetrahydride; n-butyllithium; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00048a046

Reference yield:

: 53215-95-5
N-(trimethylsilylmethyl)benzylamine

: 143957-53-3
Acetic acid 1-[2-(benzyl-trimethylsilanylmethyl-amino)-ethyl]-cyclohexa-2,5-dienylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / Et₃N / CH₂Cl₂ / 8 h / 25 °C

2: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 1.5 h, 2.) a) -78 deg C, b) 25 deg C, 12 h

3: LiAlH₄ / tetrahydrofuran / 0.17 h / Heating

4: Et₃N / CH₂Cl₂ / 1 h / 25 °C

With lithium aluminium tetrahydride; n-butyllithium; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00048a046

Reference yield:

: 143925-61-5
1-[(Benzyl-trimethylsilanylmethyl-carbamoyl)-methyl]-cyclohexa-2,5-dienecarboxylic acid methyl ester

: 143957-53-3
Acetic acid 1-[2-(benzyl-trimethylsilanylmethyl-amino)-ethyl]-cyclohexa-2,5-dienylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / tetrahydrofuran / 0.17 h / Heating

2: Et₃N / CH₂Cl₂ / 1 h / 25 °C

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00048a046