(D,L) N-(4-methoxybenzenesulfonyl)-O-(2-tetrahydropyranyl)serine, methyl ester

Base Information

• Chemical Name: (D,L) N-(4-methoxybenzenesulfonyl)-O-(2-tetrahydropyranyl)serine, methyl ester
• CAS No.: 233755-00-5
• Molecular Formula: C₁₆H₂₃NO₇S
• Molecular Weight: 373.427

Synonyms:(D,L) N-(4-methoxybenzenesulfonyl)-O-(2-tetrahydropyranyl)serine, methyl ester

Chemical Property of (D,L) N-(4-methoxybenzenesulfonyl)-O-(2-tetrahydropyranyl)serine, methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of (D,L) N-(4-methoxybenzenesulfonyl)-O-(2-tetrahydropyranyl)serine, methyl ester

There total 1 articles about (D,L) N-(4-methoxybenzenesulfonyl)-O-(2-tetrahydropyranyl)serine, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4-dihydro-2H-pyran (110-87-2) + methyl 3-hydroxy-2-(4-methoxybenzenesulfonylamino)propionate (85622-74-8) → (D,L) N-(4-methoxybenzenesulfonyl)-O-(2-tetrahydropyranyl)serine, methyl ester (233755-00-5)

Guidance literature:

With toluene-4-sulfonic acid; In tetrahydrofuran; Heating / reflux;

Reference yield:

(D,L) N-(4-methoxybenzenesulfonyl)-O-(2-tetrahydropyranyl)serine, methyl ester (233755-00-5) + 5-methyl-2-nitrobenzyl alcohol (66424-92-8) → methyl 3-[(2-tetrahydropyranyl)oxy]-2-[(-4-methoxybenzenesulfonyl)-(5-methyl-2-nitrobenzyl)amino]propionate (233755-15-2)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃;

Reference yield:

(D,L) N-(4-methoxybenzenesulfonyl)-O-(2-tetrahydropyranyl)serine, methyl ester (233755-00-5) + (4-chloro-2-nitrophenyl)methanol (22996-18-5) → methyl 3-[(2-tetrahydropyranyl)oxy]-2-[(4-methoxybenzenesulfonyl)-(2-nitro-4-chlorobenzyl)amino]propionate (232953-53-6)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃;

upstream raw materials:

3,4-dihydro-2H-pyran

methyl 3-hydroxy-2-(4-methoxybenzenesulfonylamino)propionate

Downstream raw materials:

methyl 3-[(2-tetrahydropyranyl)oxy]-2-[(-4-methoxybenzenesulfonyl)-(5-methyl-2-nitrobenzyl)amino]propionate

methyl 3-[(2-tetrahydropyranyl)oxy]-2-[(4-methoxybenzenesulfonyl)-(2-nitro-4-chlorobenzyl)amino]propionate

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