C₃₀H₃₂BrN₅O₂S

Base Information

• Chemical Name: C₃₀H₃₂BrN₅O₂S
• CAS No.: 1085938-15-3
• Molecular Formula: C₃₀H₃₂BrN₅O₂S
• Molecular Weight: 606.586
• Mol file: 1085938-15-3.mol

Synonyms:C₃₀H₃₂BrN₅O₂S

Chemical Property of C₃₀H₃₂BrN₅O₂S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₃₂BrN₅O₂S

There total 11 articles about C₃₀H₃₂BrN₅O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

{3-[[1-(2-bromo-5-oxo-6-thiophen-2-ylmethyl-5,6-dihydro-1H-1,6,8-triaza-cyclopenta[b]naphthalen-7-yl)-2-methyl-propyl]-(4-methyl-benzoyl)-amino]-propyl}-carbamic acid tert-butyl ester (1085940-85-7) → C30H32BrN5O2S (1085938-15-3)

Guidance literature:

With hydrogenchloride; In dichloromethane; at 0 - 20 ℃; for 3h;

Reference yield:

(E)-methyl 5-(2-(dimethylamino)vinyl)-2,4-dinitrobenzoate → C30H32BrN5O2S (1085938-15-3)

Guidance literature:

Multi-step reaction with 10 steps

1.1: hydrogen / palladium 10% on activated carbon / ethanol / 3102.97 Torr

2.1: N,N-dimethyl-formamide / 25 h / 20 °C

3.1: lithium hydroxide; water / tetrahydrofuran / 16 h / 80 °C

3.2: pH 3 - 4

4.1: 30 h / Heating / reflux

5.1: toluene / 88.8 h / Heating / reflux

5.2: 6 h / 140 °C

5.3: pH 8 - 9

6.1: acetic acid / 24 h / Heating / reflux

7.1: bromine; sodium acetate / acetic acid / 5.17 h / 20 °C

8.1: dichloromethane / 7 h / 20 - 90 °C

9.1: triethylamine / dichloromethane / 23 h / 0 - 20 °C

10.1: hydrogenchloride / dichloromethane / 3 h / 0 - 20 °C

With hydrogenchloride; lithium hydroxide; water; hydrogen; bromine; sodium acetate; acetic acid; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; acetic acid; N,N-dimethyl-formamide; toluene;

Reference yield:

methyl 5-methyl-2,4-dinitrobenzoate (52090-25-2) → C30H32BrN5O2S (1085938-15-3)

Guidance literature:

Multi-step reaction with 11 steps

1.1: toluene / 96 h / Heating / reflux

2.1: hydrogen / palladium 10% on activated carbon / ethanol / 3102.97 Torr

3.1: N,N-dimethyl-formamide / 25 h / 20 °C

4.1: lithium hydroxide; water / tetrahydrofuran / 16 h / 80 °C

4.2: pH 3 - 4

5.1: 30 h / Heating / reflux

6.1: toluene / 88.8 h / Heating / reflux

6.2: 6 h / 140 °C

6.3: pH 8 - 9

7.1: acetic acid / 24 h / Heating / reflux

8.1: bromine; sodium acetate / acetic acid / 5.17 h / 20 °C

9.1: dichloromethane / 7 h / 20 - 90 °C

10.1: triethylamine / dichloromethane / 23 h / 0 - 20 °C

11.1: hydrogenchloride / dichloromethane / 3 h / 0 - 20 °C

With hydrogenchloride; lithium hydroxide; water; hydrogen; bromine; sodium acetate; acetic acid; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; acetic acid; N,N-dimethyl-formamide; toluene;

upstream raw materials:

{3-[[1-(2-bromo-5-oxo-6-thiophen-2-ylmethyl-5,6-dihydro-1H-1,6,8-triaza-cyclopenta[b]naphthalen-7-yl)-2-methyl-propyl]-(4-methyl-benzoyl)-amino]-propyl}-carbamic acid tert-butyl ester

methyl 6-amino-1H-indole-5-carboxylate

6-(3-methyl-butyrylamino)-1H-indole-5-carboxylic acid methyl ester

2-isobutyl-3-(thiophen-2-ylmethyl)-3H-pyrrolo[3,2-g]quinazolin-4(8H)-one