(2R,3R)-tert-butyl 3-(tert-butoxycarbonylamino)-3-(4-methoxyphenyl)-2-methyl-2-nitro-propanoate

Base Information

• Chemical Name: (2R,3R)-tert-butyl 3-(tert-butoxycarbonylamino)-3-(4-methoxyphenyl)-2-methyl-2-nitro-propanoate
• CAS No.: 1010805-23-8
• Molecular Formula: C₂₀H₃₀N₂O₇
• Molecular Weight: 410.467

Synonyms:(2R,3R)-tert-butyl 3-(tert-butoxycarbonylamino)-3-(4-methoxyphenyl)-2-methyl-2-nitro-propanoate

Chemical Property of (2R,3R)-tert-butyl 3-(tert-butoxycarbonylamino)-3-(4-methoxyphenyl)-2-methyl-2-nitro-propanoate

Chemical Property:

Purity/Quality:

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Technology Process of (2R,3R)-tert-butyl 3-(tert-butoxycarbonylamino)-3-(4-methoxyphenyl)-2-methyl-2-nitro-propanoate

There total 4 articles about (2R,3R)-tert-butyl 3-(tert-butoxycarbonylamino)-3-(4-methoxyphenyl)-2-methyl-2-nitro-propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2-nitropropanoic acid tert-butyl ester (18598-92-0) + tert-butyl 4-methoxybenzylidenecarbamate (743430-44-6) → (2R,3R)-tert-butyl 3-(tert-butoxycarbonylamino)-3-(4-methoxyphenyl)-2-methyl-2-nitro-propanoate (1010805-23-8) + (2RS,3SR)-tert-butyl 3-(tert-butoxycarbonylamino)-3-(4-methoxyphenyl)-2-methyl-2-nitro-propanoate

Guidance literature:

With 4 A molecular sieve; nickel complex of (R)-Schiff base, derivatives of binaphthyl; In tetrahydrofuran; at 0 ℃; for 12h;

DOI:10.1021/ja710398q

Reference yield:

2-nitropropanoic acid tert-butyl ester (18598-92-0) + tert-butyl 4-methoxybenzylidenecarbamate (743430-44-6) → (2R,3R)-tert-butyl 3-(tert-butoxycarbonylamino)-3-(4-methoxyphenyl)-2-methyl-2-nitro-propanoate (1010805-23-8) + C20H30N2O7 + C20H30N2O7 (1044200-49-8)

Guidance literature:

With C₅₆H₄₁Cl₂NO₂; In toluene; at 0 ℃; for 9h;

DOI:10.1021/ja8041004

Reference yield:

→ (2R,3R)-tert-butyl 3-(tert-butoxycarbonylamino)-3-(4-methoxyphenyl)-2-methyl-2-nitro-propanoate (1010805-23-8) + (2RS,3SR)-tert-butyl 3-(tert-butoxycarbonylamino)-3-(4-methoxyphenyl)-2-methyl-2-nitro-propanoate

Guidance literature:

upstream raw materials:

2-nitropropanoic acid tert-butyl ester

tert-butyl 4-methoxybenzylidenecarbamate

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