2',4'-Dihydroxy-3'-methyl-5'-nitroacetophenone

Base Information

Chemical Name:2',4'-Dihydroxy-3'-methyl-5'-nitroacetophenone
CAS No.:118824-94-5
Molecular Formula:C₉H₉NO₅
Molecular Weight:211.174
Hs Code.:
European Community (EC) Number:661-793-2

Synonyms:2',4'-DIHYDROXY-3'-METHYL-5'-NITROACETOPHENONE;AKOS024324792

Suppliers and Price of 2',4'-Dihydroxy-3'-methyl-5'-nitroacetophenone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2',4'-Dihydroxy-3'-methyl-5'-nitroacetophenone

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:1
Exact Mass:211.04807239
Heavy Atom Count:15
Complexity:274

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C(=CC(=C1O)[N+](=O)[O-])C(=O)C)O

Technology Process of 2',4'-Dihydroxy-3'-methyl-5'-nitroacetophenone

There total 3 articles about 2',4'-Dihydroxy-3'-methyl-5'-nitroacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 108-24-7
acetic anhydride

: 65938-75-2
1,3-dihydroxy-2-methyl-4-nitrobenzene

: 118824-94-5
2',4'-Dihydroxy-3'-methyl-5'-nitroacetophenone

Guidance literature:: aluminium trichloride; In nitrobenzene; at 80 ℃; for 7h;
DOI:10.1039/P19880001823

Reference yield:

: 65882-00-0
2-methyl-4-nitrosobenzene-1,3-diol

: 118824-94-5
2',4'-Dihydroxy-3'-methyl-5'-nitroacetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / nitric acid / H₂O / Ambient temperature

2: 73 percent / aluminium chloride / nitrobenzene / 7 h / 80 °C

With nitric acid; aluminium trichloride; In water; nitrobenzene;
DOI:10.1039/P19880001823

Reference yield:

: 608-25-3
2-methylbenzene-1,3-diol

: 118824-94-5
2',4'-Dihydroxy-3'-methyl-5'-nitroacetophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / sodium nitrite, sulphuric acid / H₂O

2: 64 percent / nitric acid / H₂O / Ambient temperature

3: 73 percent / aluminium chloride / nitrobenzene / 7 h / 80 °C

With sulfuric acid; nitric acid; sodium nitrite; aluminium trichloride; In water; nitrobenzene;
DOI:10.1039/P19880001823