2-[(4-{benzyl-[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-2-hydroxybutylimino)methyl]phenol

Base Information

Chemical Name:2-[(4-{benzyl-[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-2-hydroxybutylimino)methyl]phenol
CAS No.:402921-49-7
Molecular Formula:C₃₂H₃₇N₅O₂
Molecular Weight:523.678
Hs Code.:

Synonyms:2-[(4-{benzyl-[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-2-hydroxybutylimino)methyl]phenol

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Chemical Property of 2-[(4-{benzyl-[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-2-hydroxybutylimino)methyl]phenol

Chemical Property:

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Technology Process of 2-[(4-{benzyl-[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-2-hydroxybutylimino)methyl]phenol

There total 11 articles about 2-[(4-{benzyl-[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-2-hydroxybutylimino)methyl]phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 90-02-8
salicylaldehyde

: 402921-68-0
1-amino-4-{benzyl-[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}butan-2-ol

: 402921-49-7
2-[(4-{benzyl-[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-2-hydroxybutylimino)methyl]phenol

Guidance literature:: In benzene; at 40 ℃; for 1h;
DOI:10.1039/b103164n

Reference yield:

: 189440-33-3
(2-aminoethyl)bis(2-pyridylmethyl)amine

: 402921-49-7
2-[(4-{benzyl-[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-2-hydroxybutylimino)methyl]phenol

Guidance literature:: Multi-step reaction with 6 steps

1: 100 percent / MgSO₄ / CH₂Cl₂ / 3 h / 20 °C

2: 91 percent / NaBH₄ / acetonitrile; acetic acid; ethanol / 18 h / 20 °C

3: 100 percent / methanol / 18 h / 20 °C

4: NaBH₄ / methanol / 5 h / 5 °C

5: 3.0 g / aq. HCl / 18 h / 20 °C

6: 100 percent / benzene / 1 h / 40 °C

With hydrogenchloride; sodium tetrahydroborate; magnesium sulfate; In methanol; ethanol; dichloromethane; acetic acid; acetonitrile; benzene; 3: Michael addition;
DOI:10.1039/b103164n

Reference yield:

: 1121-60-4
pyridine-2-carbaldehyde

: 402921-49-7
2-[(4-{benzyl-[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-2-hydroxybutylimino)methyl]phenol

Guidance literature:: Multi-step reaction with 10 steps

1: 100 percent / MgSO₄ / CH₂Cl₂ / 3 h / 20 °C

2: 73 percent / NaBH₄ / acetonitrile; ethanol; acetic acid / 18 h / 20 °C

3: 68 percent / K₂CO₃; KI / acetonitrile / 24 h / Heating

4: 68 percent / hydrazine monohydrate / ethanol / 3 h / Heating

5: 100 percent / MgSO₄ / CH₂Cl₂ / 3 h / 20 °C

6: 91 percent / NaBH₄ / acetonitrile; acetic acid; ethanol / 18 h / 20 °C

7: 100 percent / methanol / 18 h / 20 °C

8: NaBH₄ / methanol / 5 h / 5 °C

9: 3.0 g / aq. HCl / 18 h / 20 °C

10: 100 percent / benzene / 1 h / 40 °C

With hydrogenchloride; sodium tetrahydroborate; magnesium sulfate; potassium carbonate; hydrazine hydrate; potassium iodide; In methanol; ethanol; dichloromethane; acetic acid; acetonitrile; benzene; 7: Michael addition;
DOI:10.1039/b103164n