2-(4-(benzo[d]oxazol-2-yl)-1-methylpiperidin-4-ylamino)phenyl phenylcarbamate

Base Information

Chemical Name:2-(4-(benzo[d]oxazol-2-yl)-1-methylpiperidin-4-ylamino)phenyl phenylcarbamate
CAS No.:1572383-52-8
Molecular Formula:C₂₆H₂₆N₄O₃
Molecular Weight:442.517
Hs Code.:

Synonyms:2-(4-(benzo[d]oxazol-2-yl)-1-methylpiperidin-4-ylamino)phenyl phenylcarbamate

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Chemical Property of 2-(4-(benzo[d]oxazol-2-yl)-1-methylpiperidin-4-ylamino)phenyl phenylcarbamate

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Technology Process of 2-(4-(benzo[d]oxazol-2-yl)-1-methylpiperidin-4-ylamino)phenyl phenylcarbamate

There total 7 articles about 2-(4-(benzo[d]oxazol-2-yl)-1-methylpiperidin-4-ylamino)phenyl phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1572383-01-7
2-(4-(benzo[d]oxazol-2-yl)-1-methylpiperidin-4-ylamino)phenol

: 103-71-9
phenyl isocyanate

: 1572383-52-8
2-(4-(benzo[d]oxazol-2-yl)-1-methylpiperidin-4-ylamino)phenyl phenylcarbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 35 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ol500328t

Reference yield:

: 95-55-6
2-amino-phenol

: 1572383-52-8
2-(4-(benzo[d]oxazol-2-yl)-1-methylpiperidin-4-ylamino)phenyl phenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluorormethanesulfonic acid / 2,2,2-trifluoroethanol / 1 h / 55 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 35 °C / Inert atmosphere

With trifluorormethanesulfonic acid; N-ethyl-N,N-diisopropylamine; In dichloromethane; 2,2,2-trifluoroethanol;
DOI:10.1021/ol500328t

Reference yield:

: 1445-73-4
1-Methyl-4-piperidone

: 1572383-52-8
2-(4-(benzo[d]oxazol-2-yl)-1-methylpiperidin-4-ylamino)phenyl phenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluorormethanesulfonic acid / 2,2,2-trifluoroethanol / 1 h / 55 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 35 °C / Inert atmosphere

With trifluorormethanesulfonic acid; N-ethyl-N,N-diisopropylamine; In dichloromethane; 2,2,2-trifluoroethanol;
DOI:10.1021/ol500328t