Technology Process of methyl 3-(3'.5'-dihydroxyphenyl)propanoate
There total 7 articles about methyl 3-(3'.5'-dihydroxyphenyl)propanoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
ethanol;
DOI:10.1021/ja060062a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 96 percent / morpholine; AcOH / Heating
2: 95 percent / p-toluenesulfonic acid monohydrate / 24 h / Heating
3: 83 percent / H2 / Pd/C / ethanol
With
morpholine; hydrogen; toluene-4-sulfonic acid; acetic acid;
palladium on activated charcoal;
In
ethanol;
1: Knoevenagel condensation;
DOI:10.1021/ja060062a
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 96 percent / K2CO3 / dimethylformamide / 8 h / 75 °C
2: 92 percent / LiAlH4 / tetrahydrofuran / 0 - 20 °C
3: pyridinium chlorochromate / CH2Cl2 / 20 °C
4: 96 percent / morpholine; AcOH / Heating
5: 95 percent / p-toluenesulfonic acid monohydrate / 24 h / Heating
6: 83 percent / H2 / Pd/C / ethanol
With
morpholine; lithium aluminium tetrahydride; hydrogen; potassium carbonate; toluene-4-sulfonic acid; acetic acid; pyridinium chlorochromate;
palladium on activated charcoal;
In
tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
4: Knoevenagel condensation;
DOI:10.1021/ja060062a
