(2S)-benzyl 4--2-<<(1,1-dimethylethoxy)carbonyl>amino>butanoate

Base Information

Chemical Name:(2S)-benzyl 4--2-<<(1,1-dimethylethoxy)carbonyl>amino>butanoate
CAS No.:158534-33-9
Molecular Formula:C₂₇H₃₅N₃O₈
Molecular Weight:529.59
Hs Code.:

(2S)-benzyl 4-<N-(benzyloxy)-N'-(ethoxycarbonyl)ureido>-2-<<(1,1-dimethylethoxy)carbonyl>amino>butanoate

Synonyms:(2S)-benzyl 4--2-<<(1,1-dimethylethoxy)carbonyl>amino>butanoate

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Chemical Property of (2S)-benzyl 4--2-<<(1,1-dimethylethoxy)carbonyl>amino>butanoate

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Technology Process of (2S)-benzyl 4--2-<<(1,1-dimethylethoxy)carbonyl>amino>butanoate

There total 3 articles about (2S)-benzyl 4--2-<<(1,1-dimethylethoxy)carbonyl>amino>butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 19617-43-7
ethoxycarbonylisocyanate

: 158534-32-8
(S)-benzyl-4-<(O-benzylhydroxy)amino>-2-<<(1,1-dimethylethoxy)carbonyl>amino>butanoate

: 158534-33-9
(2S)-benzyl 4--2-<<(1,1-dimethylethoxy)carbonyl>amino>butanoate

Guidance literature:: In tetrahydrofuran; for 0.0166667h;
DOI:10.1021/jm00049a013

Reference yield:

: 622-33-3
N-benzyloxyamine

: 158534-33-9
(2S)-benzyl 4--2-<<(1,1-dimethylethoxy)carbonyl>amino>butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / NaBH₃CN, HCl / methanol; dioxane / 48 h / Ambient temperature

2: 90 percent / tetrahydrofuran / 0.02 h

With hydrogenchloride; sodium cyanoborohydride; In tetrahydrofuran; 1,4-dioxane; methanol;
DOI:10.1021/jm00049a013

Reference yield:

: 124994-66-7
(S)-benzyl-4-oxo-2-<<(1,1-dimethylethoxy)carbonyl>amino>butanoate

: 158534-33-9
(2S)-benzyl 4--2-<<(1,1-dimethylethoxy)carbonyl>amino>butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / NaBH₃CN, HCl / methanol; dioxane / 48 h / Ambient temperature

2: 90 percent / tetrahydrofuran / 0.02 h

With hydrogenchloride; sodium cyanoborohydride; In tetrahydrofuran; 1,4-dioxane; methanol;
DOI:10.1021/jm00049a013