C₃₁H₃₈O₃

Base Information

• Chemical Name: C₃₁H₃₈O₃
• CAS No.: 1192826-30-4
• Molecular Formula: C₃₁H₃₈O₃
• Molecular Weight: 458.641
• Mol file: 1192826-30-4.mol

Synonyms:C₃₁H₃₈O₃

Chemical Property of C₃₁H₃₈O₃

Chemical Property:

Purity/Quality:

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Technology Process of C₃₁H₃₈O₃

There total 1 articles about C₃₁H₃₈O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

4-(9-hydroxynonyl)-1,3-dioxolane (1192826-52-0) + trityl chloride (76-83-5) → C31H38O3 (1192826-30-4)

Guidance literature:

With dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1021/ol902088b

Reference yield: 86.0%

C31H38O3 (1192826-30-4) → 11-(triphenylmethyloxy)undecane-1,2-diol (202645-90-7)

Guidance literature:

C₃₁H₃₈O₃; With [2,2]bipyridinyl; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;

With hydrogenchloride; water; In diethyl ether; at 20 ℃; for 4.5h;

DOI:10.1248/cpb.58.426

Reference yield:

[2,2]bipyridinyl (366-18-7) + C31H38O3 (1192826-30-4) + triethylsilyl trifluoromethyl sulfonate (79271-56-0) → CF3O3S(1-)*C47H61N2O3Si(1+)

Guidance literature:

In dichloromethane; at 0 ℃; for 0.5h; regioselective reaction; Inert atmosphere;

DOI:10.1021/ol902088b

upstream raw materials:

4-(9-hydroxynonyl)-1,3-dioxolane

trityl chloride

Downstream raw materials:

11-(triphenylmethyloxy)undecane-1,2-diol