C₁₇H₂₀Cl₂O₃

Base Information

Chemical Name:C₁₇H₂₀Cl₂O₃
CAS No.:1346010-25-0
Molecular Formula:C₁₇H₂₀Cl₂O₃
Molecular Weight:343.25
Hs Code.:

C<sub>17</sub>H<sub>20</sub>Cl<sub>2</sub>O<sub>3</sub>

Synonyms:C₁₇H₂₀Cl₂O₃

Suppliers and Price of C₁₇H₂₀Cl₂O₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₇H₂₀Cl₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₇H₂₀Cl₂O₃

There total 9 articles about C₁₇H₂₀Cl₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1346010-18-1
C₁₁H₁₈O₃

: 2123-28-6
1,2-dichloro-3-vinylbenzene

: 1346010-25-0
C₁₇H₂₀Cl₂O₃

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; for 24h; diastereoselective reaction; Reflux; Inert atmosphere;
DOI:10.1039/c1ob06039b

Reference yield:

: 1346010-21-6
C₂₃H₃₈O₇SSi

: 1346010-25-0
C₁₇H₂₀Cl₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 2.25 h / -20 - 30 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 - 30 °C

3: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / acetonitrile / 1 h / 100 °C

4: tetrahydrofuran / 2 h / -20 - 0 °C / Inert atmosphere

5: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 24 h / Reflux; Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; lithium aluminium tetrahydride; tetrabutyl ammonium fluoride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dichloromethane; acetonitrile; 4: Wittig reaction;
DOI:10.1039/c1ob06039b

Reference yield:

: 1346010-20-5
C₁₆H₃₂O₄Si

: 1346010-25-0
C₁₇H₂₀Cl₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 - 30 °C

2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / acetonitrile / 1 h / 100 °C

3: tetrahydrofuran / 2 h / -20 - 0 °C / Inert atmosphere

4: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 24 h / Reflux; Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; tetrabutyl ammonium fluoride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dichloromethane; acetonitrile; 3: Wittig reaction;
DOI:10.1039/c1ob06039b