N,N-dihydroxybenzene-1,3-dicarboximidoyl dichloride

Base Information

• Chemical Name: N,N-dihydroxybenzene-1,3-dicarboximidoyl dichloride
• CAS No.: 18728-47-7
• Molecular Formula: C₈H₆Cl₂N₂O₂
• Molecular Weight: 233.054
• Mol file: 18728-47-7.mol

Synonyms:N,N-dihydroxybenzene-1,3-dicarboximidoyl dichloride

Chemical Property of N,N-dihydroxybenzene-1,3-dicarboximidoyl dichloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N-dihydroxybenzene-1,3-dicarboximidoyl dichloride

There total 4 articles about N,N-dihydroxybenzene-1,3-dicarboximidoyl dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

benzene-1,3-dicarboxladehyde dioxime (46133-07-7) → N,N-dihydroxybenzene-1,3-dicarboximidoyl dichloride (18728-47-7)

Guidance literature:

With N-chloro-succinimide;

DOI:10.1021/ja00128a042

Reference yield:

Isophthalaldehyde (626-19-7) → N,N-dihydroxybenzene-1,3-dicarboximidoyl dichloride (18728-47-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 98 percent / NH₂OH*HCl

2: 90 percent / NCS

With N-chloro-succinimide; hydroxylamine hydrochloride;

DOI:10.1021/ja00128a042

Reference yield:

Isophthalaldehyde (626-19-7) → N,N-dihydroxybenzene-1,3-dicarboximidoyl dichloride (18728-47-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 96 percent / NH₂OH*HCl; aq. NaOH / ethanol / 1 h / 0 °C

2: 87 percent / N-chlorosuccinimide / dimethylformamide / 0.33 h

With sodium hydroxide; N-chloro-succinimide; hydroxylamine hydrochloride; In ethanol; N,N-dimethyl-formamide;

DOI:10.1055/s-2001-18061

upstream raw materials:

benzene-1,3-dicarboxladehyde dioxime

Isophthalaldehyde

Downstream raw materials:

C₂₄H₄₀N₂O₄Si₄

1,3-bis(cyanooximinomethyl)benzene

1,3-bis(4-nitrofuroxan-3-yl)benzene

1,3-bis(3-nitrofuroxan-4-yl)benzene