C₅₃H₇₁FN₁₀O₂₀S

Base Information

Chemical Name:C₅₃H₇₁FN₁₀O₂₀S
CAS No.:913625-18-0
Molecular Formula:C₅₃H₇₁FN₁₀O₂₀S
Molecular Weight:1219.27
Hs Code.:

C<sub>53</sub>H<sub>71</sub>FN<sub>10</sub>O<sub>20</sub>S

Synonyms:C₅₃H₇₁FN₁₀O₂₀S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₃H₇₁FN₁₀O₂₀S

Chemical Property:

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Technology Process of C₅₃H₇₁FN₁₀O₂₀S

There total 14 articles about C₅₃H₇₁FN₁₀O₂₀S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 913625-17-9
2-{4-[(2,4-diamino-pteridin-6-ylmethyl)-methyl-amino]-benzoylamino}-4-(5-{2-[3,4,5-triacetoxy-6-(4,5,6-triacetoxy-2-acetoxymethyl-tetrahydro-pyran-3-yloxy)-tetrahydro-pyran-2-ylmethylsulfanyl]-ethylcarbamoyl}-pentylcarbamoyl)-butyric acid methyl ester

: 913625-18-0
C₅₃H₇₁FN₁₀O₂₀S

Guidance literature:: With pyridine; hydrogen fluoride; at 20 ℃; for 2h;
DOI:10.1016/j.bmc.2006.06.034

Reference yield:

: 913625-16-8
6-((S)-4-{4-[(2,4-Diamino-pteridin-6-ylmethyl)-methyl-amino]-benzoylamino}-4-methoxycarbonyl-butyrylamino)-hexanoic acid

: 913625-18-0
C₅₃H₇₁FN₁₀O₂₀S

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / (benzotriazol-1-yl-oxy)tripyrrolidinophosphonium PF₆; ethyldiisopropylamine / CH₂Cl₂; dimethylformamide / 20 °C

2: 62 percent / HF; pyridine / 2 h / 20 °C

With pyridine; hydrogen fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2006.06.034

Reference yield:

: 913625-15-7
6-(4-{4-[(2,4-diamino-pteridin-6-ylmethyl)-methyl-amino]-benzoylamino}-4-methoxycarbonyl-butyrylamino)-hexanoic acid tert-butyl ester

: 913625-18-0
C₅₃H₇₁FN₁₀O₂₀S

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / trifluoroacetic acid / CH₂Cl₂ / 3 h / 20 °C

2: 60 percent / (benzotriazol-1-yl-oxy)tripyrrolidinophosphonium PF₆; ethyldiisopropylamine / CH₂Cl₂; dimethylformamide / 20 °C

3: 62 percent / HF; pyridine / 2 h / 20 °C

With pyridine; hydrogen fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2006.06.034