C₄₁H₄₃F₂N₃O₈S

Base Information

Chemical Name:C₄₁H₄₃F₂N₃O₈S
CAS No.:1033845-66-7
Molecular Formula:C₄₁H₄₃F₂N₃O₈S
Molecular Weight:775.871
Hs Code.:

C<sub>41</sub>H<sub>43</sub>F<sub>2</sub>N<sub>3</sub>O<sub>8</sub>S

Synonyms:C₄₁H₄₃F₂N₃O₈S

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Chemical Property of C₄₁H₄₃F₂N₃O₈S

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Technology Process of C₄₁H₄₃F₂N₃O₈S

There total 9 articles about C₄₁H₄₃F₂N₃O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 858104-65-1
N-{[4-((2R,3R)-1-(4-fluorophenyl)-3-{[2-(4-fluorophenyl)-2-hydroxyethyl]thio}-4-oxoazetidin-2-yl)phenoxy]acetyl}-D-serine

: 3403-25-6,75898-47-4
tert-butyl (2R)-2-amino-3-phenyl-propanoate hydrochloride

: 1033845-66-7
C₄₁H₄₃F₂N₃O₈S

Guidance literature:: N-{[4-((2R,3R)-1-(4-fluorophenyl)-3-{[2-(4-fluorophenyl)-2-hydroxyethyl]thio}-4-oxoazetidin-2-yl)phenoxy]acetyl}-D-serine; tert-butyl (2R)-2-amino-3-phenyl-propanoate hydrochloride; With 4-methyl-morpholine; In dichloromethane; at 20 ℃; for 0.0833333h;

With (1,1,1-Benzotriazol-1-yl)-1,1,3,3-tetramethyluronium tetrafluoroborate; In dichloromethane; for 72h;

Reference yield:

: 66560-19-8
ethyl 2-((2-oxo-2-phenylethyl)thio)acetate

: 1033845-66-7
C₄₁H₄₃F₂N₃O₈S

Guidance literature:: Multi-step reaction with 10 steps

1.1: toluene-4-sulfonic acid / toluene / 20 °C / Heating / reflux

2.1: lithium hydroxide; water / tetrahydrofuran / 19 h / 0 °C

2.2: pH 6

3.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0.33 h / 0 °C

3.2: 70 h / 20 °C

4.1: titanium(IV) isopropylate; titanium tetrachloride / dichloromethane / 0.5 h / 0 °C

4.2: 0.83 h / -40 - 0 °C

5.1: N,O-bis-(trimethylsilyl)-acetamide / toluene / 1 h / 90 °C

5.2: 18 h / 45 °C

6.1: methanol; water; triethylamine / 48 h / 50 °C

7.1: 4-methyl-morpholine / dichloromethane / 0.08 h

7.2: 3 h

8.1: trifluoroacetic acid / dichloromethane / 22 h

9.1: sodium tetrahydroborate / methanol

10.1: 4-methyl-morpholine / dichloromethane / 0.08 h / 20 °C

10.2: 72 h

With 4-methyl-morpholine; titanium(IV) isopropylate; methanol; dmap; lithium hydroxide; sodium tetrahydroborate; water; titanium tetrachloride; N,O-bis-(trimethylsilyl)-acetamide; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane; toluene;

Reference yield:

: 858104-07-1
ethyl {[(5,5-dimethyl-2-phenyl-1,3-dioxan-2-yl)methyl]thio}acetate

: 1033845-66-7
C₄₁H₄₃F₂N₃O₈S

Guidance literature:: Multi-step reaction with 9 steps

1.1: lithium hydroxide; water / tetrahydrofuran / 19 h / 0 °C

1.2: pH 6

2.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0.33 h / 0 °C

2.2: 70 h / 20 °C

3.1: titanium(IV) isopropylate; titanium tetrachloride / dichloromethane / 0.5 h / 0 °C

3.2: 0.83 h / -40 - 0 °C

4.1: N,O-bis-(trimethylsilyl)-acetamide / toluene / 1 h / 90 °C

4.2: 18 h / 45 °C

5.1: methanol; water; triethylamine / 48 h / 50 °C

6.1: 4-methyl-morpholine / dichloromethane / 0.08 h

6.2: 3 h

7.1: trifluoroacetic acid / dichloromethane / 22 h

8.1: sodium tetrahydroborate / methanol

9.1: 4-methyl-morpholine / dichloromethane / 0.08 h / 20 °C

9.2: 72 h

With 4-methyl-morpholine; titanium(IV) isopropylate; methanol; dmap; lithium hydroxide; sodium tetrahydroborate; water; titanium tetrachloride; N,O-bis-(trimethylsilyl)-acetamide; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; toluene;