allyl 2-<(3R)-3-acetoxytetradecanamido>-3-O-benzoyl-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

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Chemical Name:allyl 2-<(3R)-3-acetoxytetradecanamido>-3-O-benzoyl-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside
CAS No.:142140-99-6
Molecular Formula:C₃₅H₅₃NO₉
Molecular Weight:631.807
Hs Code.:

Synonyms:allyl 2-<(3R)-3-acetoxytetradecanamido>-3-O-benzoyl-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

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Chemical Property of allyl 2-<(3R)-3-acetoxytetradecanamido>-3-O-benzoyl-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

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Technology Process of allyl 2-<(3R)-3-acetoxytetradecanamido>-3-O-benzoyl-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

There total 4 articles about allyl 2-<(3R)-3-acetoxytetradecanamido>-3-O-benzoyl-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 93-97-0
benzoic acid anhydride

: 142140-98-5
allyl 2-<(3R)-3-acetoxytetradecanamido>-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

: 142140-99-6
allyl 2-<(3R)-3-acetoxytetradecanamido>-3-O-benzoyl-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

Guidance literature:: With dmap; In pyridine; at 30 ℃;
DOI:10.1016/S0008-6215(00)90547-0

Reference yield:

: 63064-48-2,116288-58-5,117299-90-8,126778-02-7,28738-44-5
allyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

: 142140-99-6
allyl 2-<(3R)-3-acetoxytetradecanamido>-3-O-benzoyl-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / Ba(OH)2*8H₂O / H₂O / 110 °C

2: 87 percent / methanol / 48 h / Ambient temperature

3: 81 percent / 4-toluenesulphonic acid / tetrahydrofuran; acetonitrile / 1 h / Ambient temperature

4: 80 percent / 4-dimethylaminopyridine / pyridine / 30 °C

With dmap; barium dihydroxide; toluene-4-sulfonic acid; In tetrahydrofuran; pyridine; methanol; water; acetonitrile;
DOI:10.1016/S0008-6215(00)90547-0

Reference yield:

: 114244-98-3
allyl 2-amino-2-deoxy-β-D-glucopyranoside

: 142140-99-6
allyl 2-<(3R)-3-acetoxytetradecanamido>-3-O-benzoyl-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / methanol / 48 h / Ambient temperature

2: 81 percent / 4-toluenesulphonic acid / tetrahydrofuran; acetonitrile / 1 h / Ambient temperature

3: 80 percent / 4-dimethylaminopyridine / pyridine / 30 °C

With dmap; toluene-4-sulfonic acid; In tetrahydrofuran; pyridine; methanol; acetonitrile;
DOI:10.1016/S0008-6215(00)90547-0