3',4'-dihydroxynomifensine

Base Information

Chemical Name:3',4'-dihydroxynomifensine
CAS No.:69275-19-0
Molecular Formula:C16H18 N2 O2
Molecular Weight:270.32632
Hs Code.:
Mol file:69275-19-0.mol

Synonyms:3',4'-Dihydroxynomifensine;4-(8-Amino-2-methyl-1,2,3,4-tetrahydroisoquinolin-4-yl)benzol-1,2-diol; SKF102341

Suppliers and Price of 3',4'-dihydroxynomifensine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 3',4'-dihydroxynomifensine

Chemical Property:

Vapor Pressure:1.68E-09mmHg at 25°C
Boiling Point:471.2°C at 760 mmHg
Flash Point:238.8°C
Density:1.283g/cm³

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3',4'-dihydroxynomifensine

There total 10 articles about 3',4'-dihydroxynomifensine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 138167-90-5
8-amino-1,2,3,4-tetrahydro-4-(3,4-dimethoxyphenyl)-2-methylisoquinoline

: 69275-19-0
3',4'-Dihydroxynomifensin

Guidance literature:: With boron tribromide; In dichloromethane; for 4h; Ambient temperature;
DOI:10.1021/jm00367a006

Reference yield:

: 15471-89-3
α-(aminomethyl)-3,4-dimethoxybenzyl alcohol hydrochloride

: 69275-19-0
3',4'-Dihydroxynomifensin

Guidance literature:: Multi-step reaction with 6 steps

1: 93 percent / triethylamine / methanol / 0.17 h / Heating

2: 80 percent / NaBH₄ / methanol / 30 h / 0 °C

3: 100 percent / formic acid / methanol; H₂O / 0.5 h / Heating

4: 77 percent / 28percent aq. NH₃, ferrous sulfate heptahydrate / methanol / 0.5 h / Heating

5: 35 percent / conc. H₂SO₄ / -10 °C

6: 30 percent / BBr₃ / CH₂Cl₂ / 4 h / Ambient temperature

With ammonium hydroxide; sodium tetrahydroborate; formic acid; sulfuric acid; boron tribromide; iron(II) sulfate; triethylamine; In methanol; dichloromethane; water;
DOI:10.1021/jm00367a006

Reference yield:

: 87351-92-6
α-<methyl>-3,4-dimethoxybenzyl alcohol

: 69275-19-0
3',4'-Dihydroxynomifensin

Guidance literature:: Multi-step reaction with 2 steps

1: 35 percent / conc. H₂SO₄ / -10 °C

2: 30 percent / BBr₃ / CH₂Cl₂ / 4 h / Ambient temperature

With sulfuric acid; boron tribromide; In dichloromethane;
DOI:10.1021/jm00367a006