trans-1-(3'-carboxy-4'-(benzyloxy)phenyl)-2-(3'',4''-dimethoxyphenyl)ethene

Base Information

Chemical Name:trans-1-(3'-carboxy-4'-(benzyloxy)phenyl)-2-(3'',4''-dimethoxyphenyl)ethene
CAS No.:150258-62-1
Molecular Formula:C₂₄H₂₂O₅
Molecular Weight:390.436
Hs Code.:

Synonyms:trans-1-(3'-carboxy-4'-(benzyloxy)phenyl)-2-(3'',4''-dimethoxyphenyl)ethene

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Chemical Property of trans-1-(3'-carboxy-4'-(benzyloxy)phenyl)-2-(3'',4''-dimethoxyphenyl)ethene

Chemical Property:

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Technology Process of trans-1-(3'-carboxy-4'-(benzyloxy)phenyl)-2-(3'',4''-dimethoxyphenyl)ethene

There total 6 articles about trans-1-(3'-carboxy-4'-(benzyloxy)phenyl)-2-(3'',4''-dimethoxyphenyl)ethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-Benzyloxy-5-[(E)-2-(3,4-dimethoxy-phenyl)-vinyl]-benzoic acid benzyl ester

: 150258-62-1
trans-1-(3'-carboxy-4'-(benzyloxy)phenyl)-2-(3'',4''-dimethoxyphenyl)ethene

Guidance literature:: With sodium hydroxide; In N,N-dimethyl-formamide; for 1h; Yield given;
DOI:10.1021/jm00072a022

Reference yield:

: 616-76-2
2-hydroxy-5-formylbenzoic acid

: 150258-62-1
trans-1-(3'-carboxy-4'-(benzyloxy)phenyl)-2-(3'',4''-dimethoxyphenyl)ethene

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / K₂CO₃ / dimethylformamide / 16 h / 110 °C

2: potassium tert-butoxide / dimethylformamide / 4.5 h / Ambient temperature

3: 10 N NaOH / dimethylformamide / 1 h

With sodium hydroxide; potassium tert-butylate; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jm00072a022

Reference yield:

: 93-03-8
(3,4-dimethoxyphenyl)methanol

: 150258-62-1
trans-1-(3'-carboxy-4'-(benzyloxy)phenyl)-2-(3'',4''-dimethoxyphenyl)ethene

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / SOCl₂, Et₃N / CH₂Cl₂ / 1.5 h / Ambient temperature

2: 99 percent / 110 °C

3: potassium tert-butoxide / dimethylformamide / 4.5 h / Ambient temperature

4: 10 N NaOH / dimethylformamide / 1 h

With sodium hydroxide; thionyl chloride; potassium tert-butylate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00072a022