Technology Process of C22H34O3Si
There total 6 articles about C22H34O3Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate; cerium(III) chloride;
In
methanol;
at -78 ℃;
for 0.5h;
DOI:10.1021/ja307497h
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: pyridinium p-toluenesulfonate / toluene / 12 h / 10 - 24 °C / Inert atmosphere
2.1: copper(l) iodide / tetrahydrofuran; diethyl ether / 0.5 h / -50 - 24 °C / Inert atmosphere
2.2: 1.5 h / -78 - 24 °C / Inert atmosphere
2.3: 12 h / 24 °C / Inert atmosphere
3.1: sodium tetrahydroborate; cerium(III) chloride / methanol / 0.5 h / -78 °C
With
sodium tetrahydroborate; copper(l) iodide; cerium(III) chloride; pyridinium p-toluenesulfonate;
In
tetrahydrofuran; methanol; diethyl ether; toluene;
DOI:10.1021/ja307497h
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: pyridinium p-toluenesulfonate / toluene / 12 h / 10 - 24 °C / Inert atmosphere
2.1: copper(l) iodide / tetrahydrofuran; diethyl ether / 0.5 h / -50 - 24 °C / Inert atmosphere
2.2: 1.5 h / -78 - 24 °C / Inert atmosphere
2.3: 12 h / 24 °C / Inert atmosphere
3.1: sodium tetrahydroborate; cerium(III) chloride / methanol / 0.5 h / -78 °C
With
sodium tetrahydroborate; copper(l) iodide; cerium(III) chloride; pyridinium p-toluenesulfonate;
In
tetrahydrofuran; methanol; diethyl ether; toluene;
DOI:10.1021/ja307497h
