Benzene, 2-(dimethoxymethyl)-1,3,5-trimethyl-

Base Information

• Chemical Name: Benzene, 2-(dimethoxymethyl)-1,3,5-trimethyl-
• CAS No.: 64761-29-1
• Molecular Formula: C12H18O2
• Molecular Weight: 194.274
• DSSTox Substance ID: DTXSID70452996
• Nikkaji Number: J2.288.803J
• Wikidata: Q82273950
• Mol file: 64761-29-1.mol

Synonyms:64761-29-1;Benzene, 2-(dimethoxymethyl)-1,3,5-trimethyl-;SCHEMBL18825706;DTXSID70452996;2,4,6-Trimethylbenzaldehyde dimethyl acetal

Chemical Property of Benzene, 2-(dimethoxymethyl)-1,3,5-trimethyl-

Chemical Property:

• XLogP3: 2.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 194.130679813
• Heavy Atom Count: 14
• Complexity: 154

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=C(C(=C1)C)C(OC)OC)C

Technology Process of Benzene, 2-(dimethoxymethyl)-1,3,5-trimethyl-

There total 4 articles about Benzene, 2-(dimethoxymethyl)-1,3,5-trimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

mesytaldehyde (487-68-3) + trimethyl orthoformate (149-73-5) → mesitaldehyde dimethylacetal (64761-29-1)

Guidance literature:

With camphor-10-sulfonic acid; In methanol; at 23 ℃; for 12h;

DOI:10.1021/ja0662467

Reference yield:

methanol (67-56-1) + mesytaldehyde (487-68-3) → mesitaldehyde dimethylacetal (64761-29-1)

Guidance literature:

With toluene-4-sulfonic acid;

DOI:10.1021/jo00400a009

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + mesytaldehyde (487-68-3) → mesitaldehyde dimethylacetal (64761-29-1)

Guidance literature:

at 100 ℃;

upstream raw materials:

methanol

mesytaldehyde

hydrogenchloride

trimethyl orthoformate

Downstream raw materials:

(2R,3S,4S,5R,6R,7R)-1-Benzoyloxy-6-<(1,1-dimethylethyl)dimethylsilyloxy>-7-(4-methoxybenzyloxy)-2,4,6-trimethyl-3,5-(2,4,6-trimethylbenzylidenedioxy)nonane

(R)-2-[(2R,4S,5S,6R)-6-{(1R,3R)-3-[(4S,5S,6R)-6-((1R,2R)-1,2-Dihydroxy-1-methyl-butyl)-5-methyl-2-oxo-[1,3]oxazinan-4-yl]-1-hydroxy-1-methyl-butyl}-5-methyl-2-(2,4,6-trimethyl-phenyl)-[1,3]dioxan-4-yl]-propionic acid methyl ester

(R)-2-[(4S,5S,6R)-6-{(1R,3R)-3-[(4S,5S,6R)-6-((1R,2R)-1,2-Dihydroxy-1-methyl-butyl)-5-methyl-2-oxo-[1,3]oxazinan-4-yl]-1-hydroxy-1-methyl-butyl}-5-methyl-2-(2,4,6-trimethyl-phenyl)-[1,3]dioxan-4-yl]-propionic acid methyl ester

2-[(4R,6S)-6-Hydroxymethyl-2-(2,4,6-trimethyl-phenyl)-[1,3]dioxan-4-ylmethyl]-oxazole-4-carboxylic acid methyl ester