(S)-(-)-1-(tert-butyldiphenylsilyloxymethyl)-2-(3,4-dimethoxyphenyl)ethylamine

Base Information

Chemical Name:(S)-(-)-1-(tert-butyldiphenylsilyloxymethyl)-2-(3,4-dimethoxyphenyl)ethylamine
CAS No.:336607-96-6
Molecular Formula:C₂₇H₃₅NO₃Si
Molecular Weight:449.665
Hs Code.:

Synonyms:(S)-(-)-1-(tert-butyldiphenylsilyloxymethyl)-2-(3,4-dimethoxyphenyl)ethylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-(-)-1-(tert-butyldiphenylsilyloxymethyl)-2-(3,4-dimethoxyphenyl)ethylamine

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Technology Process of (S)-(-)-1-(tert-butyldiphenylsilyloxymethyl)-2-(3,4-dimethoxyphenyl)ethylamine

There total 5 articles about (S)-(-)-1-(tert-butyldiphenylsilyloxymethyl)-2-(3,4-dimethoxyphenyl)ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 336607-94-4
(S)-(-)-[1-(tert-butyldiphenylsilyloxymethyl)-2-(3,4-dimethoxyphenyl)ethyl]carbamic acid tert-butyl ester

: 336607-96-6
(S)-(-)-1-(tert-butyldiphenylsilyloxymethyl)-2-(3,4-dimethoxyphenyl)ethylamine

Guidance literature:: With trifluoroacetic acid;
DOI:10.1016/S0040-4039(00)02319-4

Reference yield:

: 32161-30-1
(S)-3,4-dimethoxyphenylalanine

: 336607-96-6
(S)-(-)-1-(tert-butyldiphenylsilyloxymethyl)-2-(3,4-dimethoxyphenyl)ethylamine

Guidance literature:: Multi-step reaction with 5 steps

2: 92 percent

3: 87 percent / LiAlH₄

4: 95 percent

5: 86 percent / TFA

With lithium aluminium tetrahydride; trifluoroacetic acid;
DOI:10.1016/S0040-4039(00)02319-4

Reference yield:

: 105779-71-3
(S)-(-)-[2-(3,4-dimethoxyphenyl)-1-hydroxymethylethyl]carbamic acid tert-butyl ester

: 336607-96-6
(S)-(-)-1-(tert-butyldiphenylsilyloxymethyl)-2-(3,4-dimethoxyphenyl)ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / imidazole / CH₂Cl₂ / 18 h / 20 °C

2: 86 percent / CF₃CO₂H / CH₂Cl₂ / 1 h / 20 °C

With 1H-imidazole; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jo051584w