3-((3,5-bis(trifluoromethyl)benzyl)amino)-4-methoxycyclobut-3-ene-1,2-dione

Base Information

• Chemical Name: 3-((3,5-bis(trifluoromethyl)benzyl)amino)-4-methoxycyclobut-3-ene-1,2-dione
• CAS No.: 1073917-05-1
• Molecular Formula: C₁₄H₉F₆NO₃
• Molecular Weight: 353.221

Synonyms:3-((3,5-bis(trifluoromethyl)benzyl)amino)-4-methoxycyclobut-3-ene-1,2-dione

Chemical Property of 3-((3,5-bis(trifluoromethyl)benzyl)amino)-4-methoxycyclobut-3-ene-1,2-dione

Chemical Property:

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Technology Process of 3-((3,5-bis(trifluoromethyl)benzyl)amino)-4-methoxycyclobut-3-ene-1,2-dione

There total 2 articles about 3-((3,5-bis(trifluoromethyl)benzyl)amino)-4-methoxycyclobut-3-ene-1,2-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

3,4-dimethoxy-3-cyclobutene-1,2-dione (5222-73-1) + 3,5-bis-trifluoromethylbenzylamine (85068-29-7) → 3-((3,5-bis(trifluoromethyl)benzyl)amino)-4-methoxycyclobut-3-ene-1,2-dione (1073917-05-1)

Guidance literature:

In dichloromethane; at 20 ℃; for 72h; Inert atmosphere;

DOI:10.1002/adsc.201600498

Reference yield:

C10H10F5N + 3,4-dimethoxy-3-cyclobutene-1,2-dione (5222-73-1) → 3-((3,5-bis(trifluoromethyl)benzyl)amino)-4-methoxycyclobut-3-ene-1,2-dione (1073917-05-1)

Guidance literature:

In dichloromethane;

DOI:10.1002/chem.201402192

Reference yield: 86.0%

9-amino-9-deoxy-epihydroquinine (852913-53-2) + 3-((3,5-bis(trifluoromethyl)benzyl)amino)-4-methoxycyclobut-3-ene-1,2-dione (1073917-05-1) → 3-((3,5-bis(trifluoromethyl)benzyl)amino)-4-(((1S)-((2S,4S,5R)-5-ethylquinuclidin-2-yl)(6-methoxyquinolin-4-yl)methyl)amino)cyclobut-3-ene-1,2-dione (1204591-53-6,1363811-07-7)

Guidance literature:

In methanol; at 20 ℃; for 24h;

DOI:10.1039/c4ob01472c

upstream raw materials:

3,4-dimethoxy-3-cyclobutene-1,2-dione

3,5-bis-trifluoromethylbenzylamine

Downstream raw materials:

(S)-2-(((2-((3,5-bis(trifluoromethyl)benzyl)amino)-3,4-dioxocyclobut-1-en-1-yl)amino)methyl)pyrrolidin-1-ium 2,2,2-trifluoroacetate

3-((3,5-bis(trifluoromethyl)benzyl)amino)-4-(((1R,2R)-2-(dipentylamino)cyclohexyl)amino)cyclobut-3-ene-1,2-dione

3-{[3,5-bis(trifluoromethyl)benzyl]}amino-4-{[(R,R)-2-aminocyclohexyl]amino}cyclobut-3-ene-1,2-dione

3-((3,5-bis(trifluoromethyl)benzyl)amino)-4-(((1S)-(6-methoxyquinolin-4-yl)((2S,4S,5R)-5-vinylquinuclidin-2-yl)methyl)amino)cyclobut-3-ene-1,2-dione

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