15-[2-(15-allyloxy-pentadecyloxymethoxymethyl)-benzyloxymethoxy]-pentadecan-1-ol

Base Information

Chemical Name:15-[2-(15-allyloxy-pentadecyloxymethoxymethyl)-benzyloxymethoxy]-pentadecan-1-ol
CAS No.:791805-32-8
Molecular Formula:C₄₃H₇₈O₆
Molecular Weight:691.089
Hs Code.:

Synonyms:15-[2-(15-allyloxy-pentadecyloxymethoxymethyl)-benzyloxymethoxy]-pentadecan-1-ol

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Chemical Property of 15-[2-(15-allyloxy-pentadecyloxymethoxymethyl)-benzyloxymethoxy]-pentadecan-1-ol

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Technology Process of 15-[2-(15-allyloxy-pentadecyloxymethoxymethyl)-benzyloxymethoxy]-pentadecan-1-ol

There total 10 articles about 15-[2-(15-allyloxy-pentadecyloxymethoxymethyl)-benzyloxymethoxy]-pentadecan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 791805-30-6
15-[2-(15-allyloxy-pentadecyloxymethoxymethyl)-benzyloxymethoxy]-pentadecanoic acid methyl ester

: 791805-32-8
15-[2-(15-allyloxy-pentadecyloxymethoxymethyl)-benzyloxymethoxy]-pentadecan-1-ol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; Heating;
DOI:10.1021/jo0493020

Reference yield:

: 106-02-5,81031-90-5
pentadecanolide

: 791805-32-8
15-[2-(15-allyloxy-pentadecyloxymethoxymethyl)-benzyloxymethoxy]-pentadecan-1-ol

Guidance literature:: Multi-step reaction with 8 steps

1.1: 87 percent / Amberlyst A-15 / 48 h / Heating

2.1: chlorotrimethylsilane / CH₂Cl₂ / 1.33 h / 20 °C

3.1: diisopropylethylamine; tetrabutylammonium iodide / tetrahydrofuran / Heating

4.1: 10.7 g / LiAlH₄ / tetrahydrofuran / Heating

5.1: NaH / tetrahydrofuran / 1 h / 0 °C

5.2: 66 percent / tetrabutylammonium iodide / tetrahydrofuran / 4 h / Heating

6.1: 95 percent / Dowex 50WX₈-200 H⁽¹⁺⁾ / tetrahydrofuran; H₂O

7.1: 100 percent / diisopropylethylamine; tetrabutylammonium iodide / tetrahydrofuran / 6 h / Heating

8.1: 80 percent / LiAlH₄ / tetrahydrofuran / Heating

With lithium aluminium tetrahydride; chloro-trimethyl-silane; Amberlyst A-15; Dowex 50WX₈-200 H⁽¹⁺⁾; tetra-(n-butyl)ammonium iodide; sodium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jo0493020

Reference yield:

: 76529-42-5
methyl 15-hydroxypentadecanoate

: 791805-32-8
15-[2-(15-allyloxy-pentadecyloxymethoxymethyl)-benzyloxymethoxy]-pentadecan-1-ol

Guidance literature:: Multi-step reaction with 7 steps

1.1: chlorotrimethylsilane / CH₂Cl₂ / 1.33 h / 20 °C

2.1: diisopropylethylamine; tetrabutylammonium iodide / tetrahydrofuran / Heating

3.1: 10.7 g / LiAlH₄ / tetrahydrofuran / Heating

4.1: NaH / tetrahydrofuran / 1 h / 0 °C

4.2: 66 percent / tetrabutylammonium iodide / tetrahydrofuran / 4 h / Heating

5.1: 95 percent / Dowex 50WX₈-200 H⁽¹⁺⁾ / tetrahydrofuran; H₂O

6.1: 100 percent / diisopropylethylamine; tetrabutylammonium iodide / tetrahydrofuran / 6 h / Heating

7.1: 80 percent / LiAlH₄ / tetrahydrofuran / Heating

With lithium aluminium tetrahydride; chloro-trimethyl-silane; Dowex 50WX₈-200 H⁽¹⁺⁾; tetra-(n-butyl)ammonium iodide; sodium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jo0493020