1,3,6-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-7-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)xanthone

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Chemical Name:1,3,6-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-7-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)xanthone
CAS No.:1609192-28-0
Molecular Formula:C₆₂H₆₂O₂₄
Molecular Weight:1191.16
Hs Code.:

Synonyms:1,3,6-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-7-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)xanthone

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Chemical Property of 1,3,6-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-7-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)xanthone

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Technology Process of 1,3,6-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-7-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)xanthone

There total 5 articles about 1,3,6-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-7-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)xanthone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1609192-27-9
1,3,6-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-7-hydroxyxantone

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 1609192-28-0
1,3,6-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-7-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)xanthone

Guidance literature:: With tetrabutylammomium bromide; sodium hydroxide; In chloroform; at 60 ℃; for 5h; Solvent;
DOI:10.1016/j.tetlet.2014.03.129

Reference yield: 77.6%

: 1609192-27-9
1,3,6-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-7-hydroxyxantone

: 1-bromo-α-D-(2,3,4,6-tetraacetyl)glucose

: 1609192-28-0
1,3,6-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-7-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)xanthone

Guidance literature:: With tetrabutylammomium bromide; sodium hydroxide; In chloroform; at 60 ℃; for 5h; Temperature;

Reference yield:

: Mangiferin

: 1609192-28-0
1,3,6-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-7-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)xanthone

Guidance literature:: Multi-step reaction with 4 steps

1: sodium acetate / 3.5 h / 120 °C

2: potassium carbonate; potassium iodide / acetone / 13.5 h / 20 - 60 °C

3: ammonium acetate / methanol; acetone; water / 20 - 60 °C

4: tetrabutylammomium bromide; sodium hydroxide / chloroform / 5 h / 60 °C

With ammonium acetate; tetrabutylammomium bromide; sodium acetate; potassium carbonate; potassium iodide; sodium hydroxide; In methanol; chloroform; water; acetone;
DOI:10.1016/j.tetlet.2014.03.129