1,3,6-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-7-hydroxyxantone

Base Information

Chemical Name:1,3,6-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-7-hydroxyxantone
CAS No.:1609192-27-9
Molecular Formula:C₄₈H₄₄O₁₅
Molecular Weight:860.868
Hs Code.:

Synonyms:1,3,6-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-7-hydroxyxantone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3,6-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-7-hydroxyxantone

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1,3,6-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-7-hydroxyxantone

There total 6 articles about 1,3,6-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-7-hydroxyxantone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.4%

: 1609192-26-8
1,3,6-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-7-O-acetylxanthone

: 1609192-27-9
1,3,6-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-7-hydroxyxantone

Guidance literature:: With ammonium acetate; In methanol; water; acetone; at 20 - 60 ℃;
DOI:10.1016/j.tetlet.2014.03.129

Reference yield:

: Mangiferin

: 1609192-27-9
1,3,6-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-7-hydroxyxantone

Guidance literature:: Multi-step reaction with 3 steps

1: sodium acetate / 3.5 h / 120 °C

2: potassium carbonate; potassium iodide / acetone / 13.5 h / 20 - 60 °C

3: ammonium acetate / methanol; acetone; water / 20 - 60 °C

With ammonium acetate; sodium acetate; potassium carbonate; potassium iodide; In methanol; water; acetone;
DOI:10.1016/j.tetlet.2014.03.129

Reference yield:

: 100-39-0
benzyl bromide

: 1609192-27-9
1,3,6-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-7-hydroxyxantone

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / acetone / 13.5 h / 20 - 60 °C

2: ammonium acetate / methanol; acetone; water / 20 - 60 °C

With ammonium acetate; potassium carbonate; potassium iodide; In methanol; water; acetone;
DOI:10.1016/j.tetlet.2014.03.129