(S)-ethyl 2-(5-bromo-2-(methoxymethoxy)phenyl)-2-(tert-butylsulfinylimino)acetate

Base Information

Chemical Name:(S)-ethyl 2-(5-bromo-2-(methoxymethoxy)phenyl)-2-(tert-butylsulfinylimino)acetate
CAS No.:1335218-48-8
Molecular Formula:C₁₆H₂₂BrNO₅S
Molecular Weight:420.324
Hs Code.:

Synonyms:(S)-ethyl 2-(5-bromo-2-(methoxymethoxy)phenyl)-2-(tert-butylsulfinylimino)acetate

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Chemical Property of (S)-ethyl 2-(5-bromo-2-(methoxymethoxy)phenyl)-2-(tert-butylsulfinylimino)acetate

Chemical Property:

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Technology Process of (S)-ethyl 2-(5-bromo-2-(methoxymethoxy)phenyl)-2-(tert-butylsulfinylimino)acetate

There total 3 articles about (S)-ethyl 2-(5-bromo-2-(methoxymethoxy)phenyl)-2-(tert-butylsulfinylimino)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1335218-47-7
ethyl 2-(5-bromo-2-(methoxymethoxy)phenyl)-2-oxoacetate

: 343338-28-3
(S)-2-methylpropane-2-sulfinamide

: 1335218-48-8
(S)-ethyl 2-(5-bromo-2-(methoxymethoxy)phenyl)-2-(tert-butylsulfinylimino)acetate

Guidance literature:: (S)-2-methylpropane-2-sulfinamide; With 2,2-dimethylpropyl zinc iodide; In tetrahydrofuran; at 20 ℃; for 0.25h; Inert atmosphere;

ethyl 2-(5-bromo-2-(methoxymethoxy)phenyl)-2-oxoacetate; In tetrahydrofuran; for 8h; Inert atmosphere;

Reference yield:

: 615-58-7
2,4-dibromophenol

: 1335218-48-8
(S)-ethyl 2-(5-bromo-2-(methoxymethoxy)phenyl)-2-(tert-butylsulfinylimino)acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone / 0.5 h / 20 °C

1.2: 3 h / 20 °C

2.1: n-butyllithium / diethyl ether; hexane / 0.5 h / -78 °C / Inert atmosphere

2.2: 0.75 h / -78 °C / Inert atmosphere

3.1: 2,2-dimethylpropyl zinc iodide / tetrahydrofuran / 0.25 h / 20 °C / Inert atmosphere

3.2: 8 h / Inert atmosphere

With n-butyllithium; potassium carbonate; 2,2-dimethylpropyl zinc iodide; In tetrahydrofuran; diethyl ether; hexane; acetone;

Reference yield:

: 21571-52-8
2,4-dibromo-1-(methoxymethoxy)benzene

: 1335218-48-8
(S)-ethyl 2-(5-bromo-2-(methoxymethoxy)phenyl)-2-(tert-butylsulfinylimino)acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / diethyl ether; hexane / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.75 h / -78 °C / Inert atmosphere

2.1: 2,2-dimethylpropyl zinc iodide / tetrahydrofuran / 0.25 h / 20 °C / Inert atmosphere

2.2: 8 h / Inert atmosphere

With n-butyllithium; 2,2-dimethylpropyl zinc iodide; In tetrahydrofuran; diethyl ether; hexane;