5,6,11,12-tetrachloro-2-phenyl-8,9-bis(phenylamino)-1H-benzo[5,10]anthra[2,1,9-def]isoquinoline-1,3(2H)-dione

Base Information

Chemical Name:5,6,11,12-tetrachloro-2-phenyl-8,9-bis(phenylamino)-1H-benzo[5,10]anthra[2,1,9-def]isoquinoline-1,3(2H)-dione
CAS No.:1402905-26-3
Molecular Formula:C₄₀H₂₁Cl₄N₃O₂
Molecular Weight:717.438
Hs Code.:

Synonyms:5,6,11,12-tetrachloro-2-phenyl-8,9-bis(phenylamino)-1H-benzo[5,10]anthra[2,1,9-def]isoquinoline-1,3(2H)-dione

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Chemical Property of 5,6,11,12-tetrachloro-2-phenyl-8,9-bis(phenylamino)-1H-benzo[5,10]anthra[2,1,9-def]isoquinoline-1,3(2H)-dione

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Technology Process of 5,6,11,12-tetrachloro-2-phenyl-8,9-bis(phenylamino)-1H-benzo[5,10]anthra[2,1,9-def]isoquinoline-1,3(2H)-dione

There total 1 articles about 5,6,11,12-tetrachloro-2-phenyl-8,9-bis(phenylamino)-1H-benzo[5,10]anthra[2,1,9-def]isoquinoline-1,3(2H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1402905-24-1
9,10-dibromo-1,6,7,12-tetrachloro-3,4-perylenedicarboxylic acid anhydride

: 62-53-3
aniline

: 1402905-26-3
5,6,11,12-tetrachloro-2-phenyl-8,9-bis(phenylamino)-1H-benzo[5,10]anthra[2,1,9-def]isoquinoline-1,3(2H)-dione

Guidance literature:: at 180 ℃; for 5h; Inert atmosphere;
DOI:10.1021/ol302519q

Reference yield: 96.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1402905-26-3
5,6,11,12-tetrachloro-2-phenyl-8,9-bis(phenylamino)-1H-benzo[5,10]anthra[2,1,9-def]isoquinoline-1,3(2H)-dione

: 1402905-28-5
5,6,12,13-tetrachloro-1,3,9-triphenyl-2,3-dihydropyrido[3',4',5':6,7]phenaleno[1,2,3-gh]perimidine-8,10(1H,9H)-dione

Guidance literature:: With trifluoroacetic acid; In chloroform; for 1.5h; Reflux; Inert atmosphere;
DOI:10.1021/ol302519q

Reference yield:

: 1402905-26-3
5,6,11,12-tetrachloro-2-phenyl-8,9-bis(phenylamino)-1H-benzo[5,10]anthra[2,1,9-def]isoquinoline-1,3(2H)-dione

: 1402905-30-9
1,3,9-triphenyl-2,3-dihydropyrido[3',4',5':6,7]phenaleno[1,2,3-gh]perimidine-8,10(1H,9H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / chloroform / 1.5 h / Reflux; Inert atmosphere

2: potassium hydroxide / ethylene glycol / 4 h / 165 °C

With trifluoroacetic acid; potassium hydroxide; In chloroform; ethylene glycol;
DOI:10.1021/ol302519q