5,6,12,13-tetrachloro-1,3,9-triphenyl-2,3-dihydropyrido[3',4',5':6,7]phenaleno[1,2,3-gh]perimidine-8,10(1H,9H)-dione

Base Information

Chemical Name:5,6,12,13-tetrachloro-1,3,9-triphenyl-2,3-dihydropyrido[3',4',5':6,7]phenaleno[1,2,3-gh]perimidine-8,10(1H,9H)-dione
CAS No.:1402905-28-5
Molecular Formula:C₄₁H₂₁Cl₄N₃O₂
Molecular Weight:729.449
Hs Code.:

Synonyms:5,6,12,13-tetrachloro-1,3,9-triphenyl-2,3-dihydropyrido[3',4',5':6,7]phenaleno[1,2,3-gh]perimidine-8,10(1H,9H)-dione

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Chemical Property of 5,6,12,13-tetrachloro-1,3,9-triphenyl-2,3-dihydropyrido[3',4',5':6,7]phenaleno[1,2,3-gh]perimidine-8,10(1H,9H)-dione

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Technology Process of 5,6,12,13-tetrachloro-1,3,9-triphenyl-2,3-dihydropyrido[3',4',5':6,7]phenaleno[1,2,3-gh]perimidine-8,10(1H,9H)-dione

There total 1 articles about 5,6,12,13-tetrachloro-1,3,9-triphenyl-2,3-dihydropyrido[3',4',5':6,7]phenaleno[1,2,3-gh]perimidine-8,10(1H,9H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1402905-26-3
5,6,11,12-tetrachloro-2-phenyl-8,9-bis(phenylamino)-1H-benzo[5,10]anthra[2,1,9-def]isoquinoline-1,3(2H)-dione

: 1402905-28-5
5,6,12,13-tetrachloro-1,3,9-triphenyl-2,3-dihydropyrido[3',4',5':6,7]phenaleno[1,2,3-gh]perimidine-8,10(1H,9H)-dione

Guidance literature:: With trifluoroacetic acid; In chloroform; for 1.5h; Reflux; Inert atmosphere;
DOI:10.1021/ol302519q

Reference yield: 63.0%

: 1402905-28-5
5,6,12,13-tetrachloro-1,3,9-triphenyl-2,3-dihydropyrido[3',4',5':6,7]phenaleno[1,2,3-gh]perimidine-8,10(1H,9H)-dione

: 1402905-30-9
1,3,9-triphenyl-2,3-dihydropyrido[3',4',5':6,7]phenaleno[1,2,3-gh]perimidine-8,10(1H,9H)-dione

Guidance literature:: With potassium hydroxide; In ethylene glycol; at 165 ℃; for 4h;
DOI:10.1021/ol302519q

Reference yield:

: 1402905-28-5
5,6,12,13-tetrachloro-1,3,9-triphenyl-2,3-dihydropyrido[3',4',5':6,7]phenaleno[1,2,3-gh]perimidine-8,10(1H,9H)-dione

: C₃₅H₂₀N₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / ethylene glycol / 4 h / 165 °C

2.1: potassium hydroxide / tert-butyl alcohol; 1,4-dioxane / Inert atmosphere; Reflux

2.2: 5 h / Reflux

With potassium hydroxide; In 1,4-dioxane; ethylene glycol; tert-butyl alcohol;