ether adduct of tris(pentafluorophenyl)boron

Base Information

• Chemical Name: ether adduct of tris(pentafluorophenyl)boron
• CAS No.: 6867-36-3
• Molecular Formula: C₂₂H₁₀BF₁₅O
• Molecular Weight: 586.108
• Mol file: 6867-36-3.mol

Synonyms:ether adduct of tris(pentafluorophenyl)boron

Chemical Property of ether adduct of tris(pentafluorophenyl)boron

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of ether adduct of tris(pentafluorophenyl)boron

There total 1 articles about ether adduct of tris(pentafluorophenyl)boron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

diethyl ether (60-29-7,927820-24-4) + tris(pentafluorophenyl)borate (1109-15-5) → ether adduct of tris(pentafluorophenyl)boron (6867-36-3)

Guidance literature:

at 20 ℃; Inert atmosphere; Glovebox;

DOI:10.1002/ejic.202000815

Reference yield: 83.0%

ether adduct of tris(pentafluorophenyl)boron (6867-36-3) + C31H40MoO2P2 → C49H40BF15MoO2P2

Guidance literature:

In toluene; at -78 - 20 ℃; Inert atmosphere; Schlenk technique;

DOI:10.1021/jacs.8b05874

Reference yield: 75.0%

diethyl ether (60-29-7,927820-24-4) + bromopentafluorobenzene (344-04-7) + ether adduct of tris(pentafluorophenyl)boron (6867-36-3) → lithium tetrakis(pentafluorophenyl)borate ethyl etherate (538369-97-0)

Guidance literature:

bromopentafluorobenzene; With n-butyllithium; In light petroleum; diethyl ether; hexane; at -78 ℃;

diethyl ether; ether adduct of tris(pentafluorophenyl)boron; In light petroleum; hexane; at -78 ℃;

DOI:10.1016/j.ica.2009.09.013

upstream raw materials:

diethyl ether

tris(pentafluorophenyl)borate

Downstream raw materials:

PhH₂NB(C₆F₅)3

(C₆F₅)2HB*SMe₂

H₂B(C₆F₅)·SMe₂

lithium tetrakis(pentafluorophenyl)borate ethyl etherate