4-(2-chloroethyl)-5-(3,5-dimethylphenyl)-2-[1-(5-ethyl-1,3,4-oxadiazol-2-yl)-1-methylethyl]-6H-thieno[2,3-b]pyrrole

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Chemical Name:4-(2-chloroethyl)-5-(3,5-dimethylphenyl)-2-[1-(5-ethyl-1,3,4-oxadiazol-2-yl)-1-methylethyl]-6H-thieno[2,3-b]pyrrole
CAS No.:863650-02-6
Molecular Formula:C₂₃H₂₆ClN₃OS
Molecular Weight:427.998
Hs Code.:

Synonyms:4-(2-chloroethyl)-5-(3,5-dimethylphenyl)-2-[1-(5-ethyl-1,3,4-oxadiazol-2-yl)-1-methylethyl]-6H-thieno[2,3-b]pyrrole

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Chemical Property of 4-(2-chloroethyl)-5-(3,5-dimethylphenyl)-2-[1-(5-ethyl-1,3,4-oxadiazol-2-yl)-1-methylethyl]-6H-thieno[2,3-b]pyrrole

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Technology Process of 4-(2-chloroethyl)-5-(3,5-dimethylphenyl)-2-[1-(5-ethyl-1,3,4-oxadiazol-2-yl)-1-methylethyl]-6H-thieno[2,3-b]pyrrole

There total 1 articles about 4-(2-chloroethyl)-5-(3,5-dimethylphenyl)-2-[1-(5-ethyl-1,3,4-oxadiazol-2-yl)-1-methylethyl]-6H-thieno[2,3-b]pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 863649-95-0
2-[4-(2-chloroethyl)-5-(3,5-dimethylphenyl)-6H-thieno[2,3-b]pyrrol-2-yl]-2-methylpropanohydrazide

: 115-80-0
Triethyl orthopropionate

: 863650-02-6
4-(2-chloroethyl)-5-(3,5-dimethylphenyl)-2-[1-(5-ethyl-1,3,4-oxadiazol-2-yl)-1-methylethyl]-6H-thieno[2,3-b]pyrrole

Guidance literature:: 2-[4-(2-chloroethyl)-5-(3,5-dimethylphenyl)-6H-thieno[2,3-b]pyrrol-2-yl]-2-methylpropanohydrazide; Triethyl orthopropionate; With hydrogenchloride; In 1,4-dioxane; for 0.5h;

With sodium hydroxide; In 1,4-dioxane; water;

Reference yield: 8.0%

: (3S)-1-(piperidin-4-ylcarbonyl)piperidin-3-ol

: 863650-02-6
4-(2-chloroethyl)-5-(3,5-dimethylphenyl)-2-[1-(5-ethyl-1,3,4-oxadiazol-2-yl)-1-methylethyl]-6H-thieno[2,3-b]pyrrole

: (3S)-1-{[1-(2-{5-(3,5-dimethylphenyl)-2-[1-(5-ethyl-1,3,4-oxadiazol-2-yl)-1-methylethyl]-6H-thieno[2,3-b]pyrrol-4-yl}ethyl)piperidin-4-yl]carbonyl}piperidin-3-ol

Guidance literature:: With tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; at 140 ℃; for 4h; Microwave irradiation;