2-[4-(2-chloroethyl)-5-(3,5-dimethylphenyl)-6H-thieno[2,3-b]pyrrol-2-yl]-2-methylpropanohydrazide

Base Information

Chemical Name:2-[4-(2-chloroethyl)-5-(3,5-dimethylphenyl)-6H-thieno[2,3-b]pyrrol-2-yl]-2-methylpropanohydrazide
CAS No.:863649-95-0
Molecular Formula:C₂₀H₂₄ClN₃OS
Molecular Weight:389.949
Hs Code.:

Synonyms:2-[4-(2-chloroethyl)-5-(3,5-dimethylphenyl)-6H-thieno[2,3-b]pyrrol-2-yl]-2-methylpropanohydrazide

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Chemical Property of 2-[4-(2-chloroethyl)-5-(3,5-dimethylphenyl)-6H-thieno[2,3-b]pyrrol-2-yl]-2-methylpropanohydrazide

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Technology Process of 2-[4-(2-chloroethyl)-5-(3,5-dimethylphenyl)-6H-thieno[2,3-b]pyrrol-2-yl]-2-methylpropanohydrazide

There total 1 articles about 2-[4-(2-chloroethyl)-5-(3,5-dimethylphenyl)-6H-thieno[2,3-b]pyrrol-2-yl]-2-methylpropanohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 863649-99-4
pentafluorophenyl 2-[4-(2-chloroethyl)-5-(3,5-dimethylphenyl)-6H-thieno[2,3-b]pyrrol-2-yl]-2-methylpropanoate

: 863649-95-0
2-[4-(2-chloroethyl)-5-(3,5-dimethylphenyl)-6H-thieno[2,3-b]pyrrol-2-yl]-2-methylpropanohydrazide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; hydrazine; In 1,4-dioxane; at 20 ℃; for 1h;

Reference yield: 80.0%

: 863649-95-0
2-[4-(2-chloroethyl)-5-(3,5-dimethylphenyl)-6H-thieno[2,3-b]pyrrol-2-yl]-2-methylpropanohydrazide

: 124-42-5
acetamidine hydrochloride

: 4-(2-chloroethyl)-5-(3,5-dimethylphenyl)-2-[1-methyl-1-(5-methyl-4H-1,2,4-triazol-3-yl)ethyl]-6H-thieno[2,3-b]pyrrole

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; at 100 ℃; for 2h; Molecular sieve; Microwave irradiation;

Reference yield: 61.0%

: 863649-95-0
2-[4-(2-chloroethyl)-5-(3,5-dimethylphenyl)-6H-thieno[2,3-b]pyrrol-2-yl]-2-methylpropanohydrazide

: 43083-12-1
1,1,1-trimethoxybutane

: 4-(2-chloroethyl)-5-(3,5-dimethylphenyl)-2-[1-methyl-1-(5-propyl-1,3,4-oxadiazol-2-yl)ethyl]-6H-thieno[2,3-b]pyrrole

Guidance literature:: 2-[4-(2-chloroethyl)-5-(3,5-dimethylphenyl)-6H-thieno[2,3-b]pyrrol-2-yl]-2-methylpropanohydrazide; 1,1,1-trimethoxybutane; With hydrogenchloride; In 1,4-dioxane; for 0.5h;

With sodium hydroxide; In 1,4-dioxane; water;