3-[5'-(4''-methoxybenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]imino-5-nitroisatin

Base Information

Chemical Name:3-[5'-(4''-methoxybenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]imino-5-nitroisatin
CAS No.:1332462-86-8
Molecular Formula:C₁₈H₁₄N₆O₅
Molecular Weight:394.346
Hs Code.:

Synonyms:3-[5'-(4''-methoxybenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]imino-5-nitroisatin

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Chemical Property of 3-[5'-(4''-methoxybenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]imino-5-nitroisatin

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Technology Process of 3-[5'-(4''-methoxybenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]imino-5-nitroisatin

There total 4 articles about 3-[5'-(4''-methoxybenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]imino-5-nitroisatin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 3-(4-methoxybenzyl)-4-amino-4,5-dihydro-1H-1,2,4-triazole-5-one

: 611-09-6
5-nitroisatin

: 1332462-86-8
3-[5'-(4''-methoxybenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]imino-5-nitroisatin

Guidance literature:: With acetic acid; In ethanol; at 110 ℃; for 0.05h; Microwave irradiation; Closed vessel;
DOI:10.3184/174751911X13043524455143

Reference yield:

: 100-01-6,104810-17-5
4-nitro-aniline

: 1332462-86-8
3-[5'-(4''-methoxybenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]imino-5-nitroisatin

Guidance literature:: Multi-step reaction with 3 steps

1: hydroxylamine hydrochloride; sodium sulfate

2: acetic acid

3: acetic acid / ethanol / 0.05 h / 110 °C / Microwave irradiation; Closed vessel

With hydroxylamine hydrochloride; acetic acid; sodium sulfate; In ethanol;
DOI:10.3184/174751911X13043524455143

Reference yield:

: C₁₄H₂₀N₂O₄

: 1332462-86-8
3-[5'-(4''-methoxybenzyl)-2',4'-dihydro-1',2',4'-triazol-3'-one-4'-yl]imino-5-nitroisatin

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / water / 0.05 h / 90 °C / Microwave irradiation; Closed vessel

2: acetic acid / ethanol / 0.05 h / 110 °C / Microwave irradiation; Closed vessel

With hydrazine hydrate; acetic acid; In ethanol; water;
DOI:10.3184/174751911X13043524455143