α-<3-<<3-(2-aminophenoxy)propyl>amino>propyl>-α-isopropyl-3,4,5-trimethoxybenzeneacetonitrile

Base Information

Chemical Name:α-<3-<<3-(2-aminophenoxy)propyl>amino>propyl>-α-isopropyl-3,4,5-trimethoxybenzeneacetonitrile
CAS No.:103523-48-4
Molecular Formula:C₂₆H₃₇N₃O₄
Molecular Weight:455.597
Hs Code.:

Synonyms:α-<3-<<3-(2-aminophenoxy)propyl>amino>propyl>-α-isopropyl-3,4,5-trimethoxybenzeneacetonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-<3-<<3-(2-aminophenoxy)propyl>amino>propyl>-α-isopropyl-3,4,5-trimethoxybenzeneacetonitrile

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Technology Process of α-<3-<<3-(2-aminophenoxy)propyl>amino>propyl>-α-isopropyl-3,4,5-trimethoxybenzeneacetonitrile

There total 3 articles about α-<3-<<3-(2-aminophenoxy)propyl>amino>propyl>-α-isopropyl-3,4,5-trimethoxybenzeneacetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 103523-46-2
α-isopropyl-3,4,5-trimethoxy-α-<3-<<3-(2-nitrophenoxy)propyl>amino>propyl>benzeneacetonitrile

: 103523-48-4
α-<3-<<3-(2-aminophenoxy)propyl>amino>propyl>-α-isopropyl-3,4,5-trimethoxybenzeneacetonitrile

Guidance literature:: With hydrogen; platinum(IV) oxide; In methanol; Ambient temperature;
DOI:10.1248/cpb.36.373

Reference yield:

: 103546-10-7
3-(2-nitrophenoxy)-1-propylamine

: 103523-48-4
α-<3-<<3-(2-aminophenoxy)propyl>amino>propyl>-α-isopropyl-3,4,5-trimethoxybenzeneacetonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) NaBH₄ / 1.) EtOH, 1.5 h, reflux, 2.) EtOH, ice water, 1 h, room temp.

2: 97 percent / hydrogen / PtO₂ / methanol / Ambient temperature

With sodium tetrahydroborate; hydrogen; platinum(IV) oxide; In methanol;
DOI:10.1248/cpb.36.373

Reference yield:

: 66332-86-3
α-(2-formylethyl)-α-isopropyl-3,4,5-trimethoxybenzeneacetonitrile

: 103523-48-4
α-<3-<<3-(2-aminophenoxy)propyl>amino>propyl>-α-isopropyl-3,4,5-trimethoxybenzeneacetonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) NaBH₄ / 1.) EtOH, 1.5 h, reflux, 2.) EtOH, ice water, 1 h, room temp.

2: 97 percent / hydrogen / PtO₂ / methanol / Ambient temperature

With sodium tetrahydroborate; hydrogen; platinum(IV) oxide; In methanol;
DOI:10.1248/cpb.36.373