1,11-bis(tert-butyloxycarbonyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-3,4;8,9-dibenzo-1,6,11-triazaundecane

Base Information

• Chemical Name: 1,11-bis(tert-butyloxycarbonyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-3,4;8,9-dibenzo-1,6,11-triazaundecane
• CAS No.: 615269-55-1
• Molecular Formula: C₄₇H₅₅N₃O₁₀S₃
• Molecular Weight: 918.166

Synonyms:1,11-bis(tert-butyloxycarbonyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-3,4;8,9-dibenzo-1,6,11-triazaundecane

Chemical Property of 1,11-bis(tert-butyloxycarbonyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-3,4;8,9-dibenzo-1,6,11-triazaundecane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,11-bis(tert-butyloxycarbonyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-3,4;8,9-dibenzo-1,6,11-triazaundecane

There total 1 articles about 1,11-bis(tert-butyloxycarbonyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-3,4;8,9-dibenzo-1,6,11-triazaundecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

toluene-4-sulfonamide (70-55-3) + N-(2-bromomethylbenzyl)-N-(tert-butyloxycarbonyl)-4-methyl-benzenesulfonamide → 1,11-bis(tert-butyloxycarbonyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-3,4;8,9-dibenzo-1,6,11-triazaundecane (615269-55-1)

Guidance literature:

With potassium carbonate; In acetonitrile; for 14h; Heating;

DOI:10.1002/ejoc.200300171

Reference yield: 100.0%

1,11-bis(tert-butyloxycarbonyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-3,4;8,9-dibenzo-1,6,11-triazaundecane (615269-55-1) → 1,6,11-tris[(4-methylphenyl)sulfonyl]-3,4;8,9-dibenzo-1,6,11-triazaundecane

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 7h;

DOI:10.1002/ejoc.200300171

Reference yield:

1,11-bis(tert-butyloxycarbonyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-3,4;8,9-dibenzo-1,6,11-triazaundecane (615269-55-1) → 1,6,11-tris[(4-methylphenyl)sulfonyl]-3,4;8,9;13,14-tribenzo-1,6,11-triazacyclopentadecane

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / trifluoroacetic acid / CH₂Cl₂ / 7 h / 20 °C

2: 79 percent / potassium carbonate / acetonitrile / Heating

With potassium carbonate; trifluoroacetic acid; In dichloromethane; acetonitrile;

DOI:10.1002/ejoc.200300171

upstream raw materials:

toluene-4-sulfonamide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 615269-55-1 1,11-bis(tert-butyloxycarbonyl)-1,6,11-tris[(4-methylphenyl)sulfonyl]-3,4;8,9-dibenzo-1,6,11-triazaundecane

Send

Send

Metric Ton KG G Pound L ML

Send

Send