3,4-bis<(tert-butyldimethylsilyl)oxy>-N-methyl-N-trifluoroacetylaniline

Base Information

Chemical Name:3,4-bis<(tert-butyldimethylsilyl)oxy>-N-methyl-N-trifluoroacetylaniline
CAS No.:173043-81-7
Molecular Formula:C₂₁H₃₆F₃NO₃Si₂
Molecular Weight:463.688
Hs Code.:

Synonyms:3,4-bis<(tert-butyldimethylsilyl)oxy>-N-methyl-N-trifluoroacetylaniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-bis<(tert-butyldimethylsilyl)oxy>-N-methyl-N-trifluoroacetylaniline

Chemical Property:

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Technology Process of 3,4-bis<(tert-butyldimethylsilyl)oxy>-N-methyl-N-trifluoroacetylaniline

There total 4 articles about 3,4-bis<(tert-butyldimethylsilyl)oxy>-N-methyl-N-trifluoroacetylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 69739-34-0
t-butyldimethylsiyl triflate

: 173043-93-1
3,4-dihydroxy-N-methyl-N-trifluoroacetylaniline

: 173043-81-7
3,4-bis<(tert-butyldimethylsilyl)oxy>-N-methyl-N-trifluoroacetylaniline

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; for 12h; Ambient temperature;
DOI:10.7164/antibiotics.48.1460

Reference yield:

: 54573-21-6
N-(3,4-dimethoxyphenyl)-2,2,2-trifluoroacetamide

: 173043-81-7
3,4-bis<(tert-butyldimethylsilyl)oxy>-N-methyl-N-trifluoroacetylaniline

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / NaH / dimethylformamide / 1 h / Ambient temperature

2: 893 mg / AlCl₃, EtSH / CH₂Cl₂ / 5 h / 0 °C

3: 99 percent / 2,6-lutidine / CH₂Cl₂ / 12 h / Ambient temperature

With 2,6-dimethylpyridine; aluminium trichloride; sodium hydride; ethanethiol; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.7164/antibiotics.48.1460

Reference yield:

: 173043-92-0
3,4-dimethoxy-N-methyl-N-trifluoroacetylaniline

: 173043-81-7
3,4-bis<(tert-butyldimethylsilyl)oxy>-N-methyl-N-trifluoroacetylaniline

Guidance literature:: Multi-step reaction with 2 steps

1: 893 mg / AlCl₃, EtSH / CH₂Cl₂ / 5 h / 0 °C

2: 99 percent / 2,6-lutidine / CH₂Cl₂ / 12 h / Ambient temperature

With 2,6-dimethylpyridine; aluminium trichloride; ethanethiol; In dichloromethane;
DOI:10.7164/antibiotics.48.1460