benzyl (2R)-6-{(5S)-5-[(ethanethioylamino)methyl]-2-oxo-1,3-oxazolidin-3-yl}-2-methyl-3,4-dihydro-1(2H)-quinolinecarboxylate

Base Information

Chemical Name:benzyl (2R)-6-{(5S)-5-[(ethanethioylamino)methyl]-2-oxo-1,3-oxazolidin-3-yl}-2-methyl-3,4-dihydro-1(2H)-quinolinecarboxylate
CAS No.:312306-10-8
Molecular Formula:C₂₄H₂₇N₃O₄S
Molecular Weight:453.562
Hs Code.:

Synonyms:benzyl (2R)-6-{(5S)-5-[(ethanethioylamino)methyl]-2-oxo-1,3-oxazolidin-3-yl}-2-methyl-3,4-dihydro-1(2H)-quinolinecarboxylate

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Chemical Property of benzyl (2R)-6-{(5S)-5-[(ethanethioylamino)methyl]-2-oxo-1,3-oxazolidin-3-yl}-2-methyl-3,4-dihydro-1(2H)-quinolinecarboxylate

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Technology Process of benzyl (2R)-6-{(5S)-5-[(ethanethioylamino)methyl]-2-oxo-1,3-oxazolidin-3-yl}-2-methyl-3,4-dihydro-1(2H)-quinolinecarboxylate

There total 8 articles about benzyl (2R)-6-{(5S)-5-[(ethanethioylamino)methyl]-2-oxo-1,3-oxazolidin-3-yl}-2-methyl-3,4-dihydro-1(2H)-quinolinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65079-19-8
2-methylquinolin-6-amine

: 312306-10-8
benzyl (2R)-6-{(5S)-5-[(ethanethioylamino)methyl]-2-oxo-1,3-oxazolidin-3-yl}-2-methyl-3,4-dihydro-1(2H)-quinolinecarboxylate

Guidance literature:: Multi-step reaction with 7 steps

1: H₂; H₂SO₄ / PtO₂ / methanol

2: NaHCO₃ / acetone

3: n-BuLi / tetrahydrofuran

4: Et₃N / CH₂Cl₂

5: aq. NH₃ / acetonitrile; propan-2-ol

6: Lawesson's reagent

With Lawessons reagent; ammonium hydroxide; n-butyllithium; sulfuric acid; hydrogen; sodium hydrogencarbonate; triethylamine; platinum(IV) oxide; In tetrahydrofuran; methanol; dichloromethane; isopropyl alcohol; acetone; acetonitrile;
DOI:10.1016/j.bmcl.2003.07.029

Reference yield:

: 19172-47-5,94367-93-8
Lawessons reagent

: 312306-09-5
Benzyl (2R)-6-{(5S)-5-[(acetylamino)methyl]-2-oxo-1,3-oxazolidin-3-yl}-2-methyl-3,4-dihydro-1(2H)-quinolinecarboxylate

: 312306-10-8
benzyl (2R)-6-{(5S)-5-[(ethanethioylamino)methyl]-2-oxo-1,3-oxazolidin-3-yl}-2-methyl-3,4-dihydro-1(2H)-quinolinecarboxylate

Guidance literature:: In methanol; dichloromethane; toluene;

Reference yield:

: 613-30-9
2-methyl-6-nitroquinoline

: 312306-10-8
benzyl (2R)-6-{(5S)-5-[(ethanethioylamino)methyl]-2-oxo-1,3-oxazolidin-3-yl}-2-methyl-3,4-dihydro-1(2H)-quinolinecarboxylate

Guidance literature:: Multi-step reaction with 8 steps

1: SnCl₂*H₂O / ethanol / Heating

2: H₂; H₂SO₄ / PtO₂ / methanol

3: NaHCO₃ / acetone

4: n-BuLi / tetrahydrofuran

5: Et₃N / CH₂Cl₂

6: aq. NH₃ / acetonitrile; propan-2-ol

7: Lawesson's reagent

With Lawessons reagent; ammonium hydroxide; n-butyllithium; sulfuric acid; hydrogen; sodium hydrogencarbonate; triethylamine; tin(ll) chloride; platinum(IV) oxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; isopropyl alcohol; acetone; acetonitrile;
DOI:10.1016/j.bmcl.2003.07.029