N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl]-L-serine allyl ester

Base Information

Chemical Name:N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl]-L-serine allyl ester
CAS No.:1189021-74-6
Molecular Formula:C₈₂H₆₉NO₂₂
Molecular Weight:1420.44
Hs Code.:

Synonyms:N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl]-L-serine allyl ester

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Chemical Property of N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl]-L-serine allyl ester

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Technology Process of N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl]-L-serine allyl ester

There total 2 articles about N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl]-L-serine allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 468729-86-4
2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl trichloroacetimidate

: 136497-85-3
N-(9-fluorenylmethoxycarbonyl)-L-serine allyl ester

: 1189021-74-6
N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl]-L-serine allyl ester

Guidance literature:: 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl trichloroacetimidate; N-(9-fluorenylmethoxycarbonyl)-L-serine allyl ester; In dichloromethane; at -40 - -20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; at -40 - -20 ℃; for 3h; Inert atmosphere;
DOI:10.1055/s-0029-1216820

Reference yield: 58.0%

: 1189021-72-4
4-methylphenyl 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-1-thio-α-D-mannopyranoside

: 136497-85-3
N-(9-fluorenylmethoxycarbonyl)-L-serine allyl ester

: 1189021-74-6
N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl]-L-serine allyl ester

Guidance literature:: With N-iodo-succinimide; silver trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1055/s-0029-1216820

Reference yield: 67.0%

: 1189021-74-6
N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl]-L-serine allyl ester

: 1189021-75-7
N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl]-L-serine

Guidance literature:: N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl]-L-serine allyl ester; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; for 0.166667h; Inert atmosphere;

With phenylsilane; In dichloromethane; for 1.5h; Inert atmosphere;
DOI:10.1055/s-0029-1216820