2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl trichloroacetimidate

Base Information

Chemical Name:2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl trichloroacetimidate
CAS No.:468729-86-4
Molecular Formula:C₆₃H₅₀Cl₃NO₁₈
Molecular Weight:1215.44
Hs Code.:

Synonyms:2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl trichloroacetimidate

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Chemical Property of 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl trichloroacetimidate

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Technology Process of 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl trichloroacetimidate

There total 1 articles about 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1189021-73-5
2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranoside

: 545-06-2
trichloroacetonitrile

: 468729-86-4
2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl trichloroacetimidate

Guidance literature:: 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranoside; With potassium carbonate; In dichloromethane; at 20 ℃; for 0.166667h; Inert atmosphere;

trichloroacetonitrile; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1055/s-0029-1216820

Reference yield: 74.0%

: 468729-86-4
2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl trichloroacetimidate

: 136497-85-3
N-(9-fluorenylmethoxycarbonyl)-L-serine allyl ester

: 1189021-74-6
N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl]-L-serine allyl ester

Guidance literature:: 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl trichloroacetimidate; N-(9-fluorenylmethoxycarbonyl)-L-serine allyl ester; In dichloromethane; at -40 - -20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; at -40 - -20 ℃; for 3h; Inert atmosphere;
DOI:10.1055/s-0029-1216820

Reference yield:

: 468729-86-4
2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl trichloroacetimidate

: 1439439-54-9
phenyl 3,4-di-O-benzyl-α-D-mannopyranosyl-(1→6)-2,3,4-tri-O-benzoyl-1-thio-α-D-mannopyranoside

: C₁₁₄H₉₄O₃₂S

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -80 - 20 ℃; for 3.25h; regioselective reaction; Molecular sieve;
DOI:10.1039/c3ob40421h