N-{12-[3-(2,2-diphenyl-ethylcarbamoyl)-acryloylamino]-dodecyl}-succinamic acid 2,2-diphenyl-ethyl ester

Base Information

• Chemical Name: N-{12-[3-(2,2-diphenyl-ethylcarbamoyl)-acryloylamino]-dodecyl}-succinamic acid 2,2-diphenyl-ethyl ester
• CAS No.: 573986-13-7
• Molecular Formula: C₄₈H₅₉N₃O₅
• Molecular Weight: 758.014
• Mol file: 573986-13-7.mol

Synonyms:N-{12-[3-(2,2-diphenyl-ethylcarbamoyl)-acryloylamino]-dodecyl}-succinamic acid 2,2-diphenyl-ethyl ester

Chemical Property of N-{12-[3-(2,2-diphenyl-ethylcarbamoyl)-acryloylamino]-dodecyl}-succinamic acid 2,2-diphenyl-ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-{12-[3-(2,2-diphenyl-ethylcarbamoyl)-acryloylamino]-dodecyl}-succinamic acid 2,2-diphenyl-ethyl ester

There total 3 articles about N-{12-[3-(2,2-diphenyl-ethylcarbamoyl)-acryloylamino]-dodecyl}-succinamic acid 2,2-diphenyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

N-(12-{[(2R,3R)-3-(2,2-Diphenyl-ethylcarbamoyl)-bicyclo[2.2.1]hept-5-ene-2-carbonyl]-amino}-dodecyl)-succinamic acid 2,2-diphenyl-ethyl ester → N-{12-[3-(2,2-diphenyl-ethylcarbamoyl)-acryloylamino]-dodecyl}-succinamic acid 2,2-diphenyl-ethyl ester (573986-13-7)

Guidance literature:

at 250 ℃; for 0.333333h; under 0.01 Torr;

DOI:10.1039/b412570c

Reference yield: 76.0%

(E)-4-((2,2-diphenylethyl)amino)-4-oxobut-2-enoic acid (573986-12-6) + 2,2-diphenylethyl 4-(12-aminododecylamino)-4-oxobutanoate (900524-88-1) → N-{12-[3-(2,2-diphenyl-ethylcarbamoyl)-acryloylamino]-dodecyl}-succinamic acid 2,2-diphenyl-ethyl ester (573986-13-7)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide;

DOI:10.1002/anie.200250745

Reference yield:

N-{12-[3-(2,2-diphenyl-ethylcarbamoyl)-acryloylamino]-dodecyl}-succinamic acid 2,2-diphenyl-ethyl ester (573986-22-8) → N-{12-[3-(2,2-diphenyl-ethylcarbamoyl)-acryloylamino]-dodecyl}-succinamic acid 2,2-diphenyl-ethyl ester (573986-13-7)

Guidance literature:

In 1,1,2,2-tetrachloroethane; at 120 ℃;

DOI:10.1002/anie.200250745

upstream raw materials:

(E)-4-((2,2-diphenylethyl)amino)-4-oxobut-2-enoic acid

2,2-diphenylethyl 4-(12-aminododecylamino)-4-oxobutanoate

N-{12-[3-(2,2-diphenyl-ethylcarbamoyl)-acryloylamino]-dodecyl}-succinamic acid 2,2-diphenyl-ethyl ester

Downstream raw materials:

N-{12-[3-(2,2-diphenyl-ethylcarbamoyl)-acryloylamino]-dodecyl}-succinamic acid 2,2-diphenyl-ethyl ester