dicyclohexylboranyl-acetic acid 2,6-diisopropyl-phenyl ester

Base Information

Chemical Name:dicyclohexylboranyl-acetic acid 2,6-diisopropyl-phenyl ester
CAS No.:467213-73-6
Molecular Formula:C₂₆H₄₁BO₂
Molecular Weight:396.421
Hs Code.:

Synonyms:dicyclohexylboranyl-acetic acid 2,6-diisopropyl-phenyl ester

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Chemical Property of dicyclohexylboranyl-acetic acid 2,6-diisopropyl-phenyl ester

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Technology Process of dicyclohexylboranyl-acetic acid 2,6-diisopropyl-phenyl ester

There total 3 articles about dicyclohexylboranyl-acetic acid 2,6-diisopropyl-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28000-66-0
2,6-Diisopropylphenyl acetate

: 145412-54-0
dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane

: 467213-73-6
dicyclohexylboranyl-acetic acid 2,6-diisopropyl-phenyl ester

: ((CH₃)2CH)2C₆H₃OC(CH₂)OB(C₆H₁₁)2

: C₃₈H₆₂B₂O₂

Guidance literature:: With triethylamine; In chloroform-d1; at 0 ℃; for 0.0833333h; Title compound not separated from byproducts.;
DOI:10.1021/ja0260014

Reference yield:

: 28000-66-0
2,6-Diisopropylphenyl acetate

: 100-52-7
benzaldehyde

: 145412-54-0
dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane

: 467213-73-6
dicyclohexylboranyl-acetic acid 2,6-diisopropyl-phenyl ester

: ((CH₃)2CH)2C₆H₃OC(CH₂)OB(C₆H₁₁)2

: C₃₃H₄₇BO₃

Guidance literature:: 2,6-Diisopropylphenyl acetate; dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane; With triethylamine; In chloroform-d1; at 0 ℃; for 0.0833333h;

benzaldehyde; In chloroform-d1; at 0 ℃; Further stages. Title compound not separated from byproducts.;
DOI:10.1021/ja0260014

Reference yield:

: 28000-66-0
2,6-Diisopropylphenyl acetate

: 145412-54-0
dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane

: 467213-73-6
dicyclohexylboranyl-acetic acid 2,6-diisopropyl-phenyl ester

: ((CH₃)2CH)2C₆H₃OC(CH₂)OB(C₆H₁₁)2

Guidance literature:: With triethylamine; In chloroform-d1; ester aws treated with c-Hex2BOSO2CF3 (1.3 equiv.) and Et3N (1.5 equiv.)in CDCl3 at 0°C; NMR monitoring; not isolated;
DOI:10.1021/ja0260014